benzyloxyacetyl fluoride

Base Information

• Chemical Name: benzyloxyacetyl fluoride
• CAS No.: 220329-77-1
• Molecular Formula: C₉H₉FO₂
• Molecular Weight: 168.168

Synonyms:benzyloxyacetyl fluoride

Chemical Property of benzyloxyacetyl fluoride

Chemical Property:

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Technology Process of benzyloxyacetyl fluoride

There total 1 articles about benzyloxyacetyl fluoride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

benzyloxyacetic acid (30379-55-6) → benzyloxyacetyl fluoride (220329-77-1)

Guidance literature:

With pyridine; trifluoro-[1,3,5]triazine; In dichloromethane; at 23 ℃; for 2h;

Reference yield: 73.0%

benzyloxyacetyl fluoride (220329-77-1) + (2S,4R)-1-benzyl-4-tert-butyldimethylsilyloxy-2-vinylpyrrolidine (156441-18-8) → (pS)E-3S,8R-1-benzyl-3-benzyloxy-8-(tert-butyldimethylsilyloxy)-2,3,4,7,8,9-tetrahydro-1H-azonin-2-one

Guidance literature:

With trimethylaluminum; potassium carbonate; In n-heptane; dichloromethane; at 0 - 20 ℃;

DOI:10.1021/jo991484o

Reference yield: 68.0%

benzyloxyacetyl fluoride (220329-77-1) + (S)-2-((E)-3-Pyrrolidin-1-yl-propenyl)-pyrrolidine-1-carboxylic acid tert-butyl ester (220329-71-5) → (S)-2-[(R)-1-((R)-1-Benzyloxy-2-oxo-2-pyrrolidin-1-yl-ethyl)-allyl]-pyrrolidine-1-carboxylic acid tert-butyl ester (220329-92-0)

Guidance literature:

With trimethylaluminum; sodium carbonate; In chloroform; toluene; at 0 - 23 ℃;

DOI:10.1055/s-1999-2530

upstream raw materials:

benzyloxyacetic acid

Downstream raw materials:

(S)-2-[(R)-1-((R)-1-Benzyloxy-2-oxo-2-pyrrolidin-1-yl-ethyl)-allyl]-pyrrolidine-1-carboxylic acid tert-butyl ester

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