O-trimethylsilyl [3-(trifluoromethyl)phenyl][2-(2-phenyl-1,1,1-trifluoroethyl)]hydroxylamine

Base Information

• Chemical Name: O-trimethylsilyl [3-(trifluoromethyl)phenyl][2-(2-phenyl-1,1,1-trifluoroethyl)]hydroxylamine
• CAS No.: 340283-88-7
• Molecular Formula: C₁₈H₁₉F₆NOSi
• Molecular Weight: 407.431

Synonyms:O-trimethylsilyl [3-(trifluoromethyl)phenyl][2-(2-phenyl-1,1,1-trifluoroethyl)]hydroxylamine

Chemical Property of O-trimethylsilyl [3-(trifluoromethyl)phenyl][2-(2-phenyl-1,1,1-trifluoroethyl)]hydroxylamine

Chemical Property:

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Technology Process of O-trimethylsilyl [3-(trifluoromethyl)phenyl][2-(2-phenyl-1,1,1-trifluoroethyl)]hydroxylamine

There total 1 articles about O-trimethylsilyl [3-(trifluoromethyl)phenyl][2-(2-phenyl-1,1,1-trifluoroethyl)]hydroxylamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

N-benzyl-4-(trifluoromethyl)aniline (405-81-2) → O-trimethylsilyl [3-(trifluoromethyl)phenyl][2-(2-phenyl-1,1,1-trifluoroethyl)]hydroxylamine (340283-88-7)

Guidance literature:

Multi-step reaction with 2 steps

1: sodium tungstate dihydrate; aq. H₂O₂ / methanol / 2 h / 0 °C

2: 72 percent / potassium t-butoxide / tetrahydrofuran / 48 h / -30 - -20 °C

With sodium tungstate; potassium tert-butylate; dihydrogen peroxide; In tetrahydrofuran; methanol;

DOI:10.1021/jo000685l

Reference yield: 92.0%

O-trimethylsilyl [3-(trifluoromethyl)phenyl][2-(2-phenyl-1,1,1-trifluoroethyl)]hydroxylamine (340283-88-7) → [3-(trifluoromethyl)phenyl][2-(2-phenyl-1,1,1-trifluoroethyl)] amine

Guidance literature:

With ammonium formate; palladium on activated charcoal; In methanol; at 20 ℃; for 4h;

DOI:10.1021/jo000685l

Reference yield: 79.0%

O-trimethylsilyl [3-(trifluoromethyl)phenyl][2-(2-phenyl-1,1,1-trifluoroethyl)]hydroxylamine (340283-88-7) → [3-(trifluoromethyl)phenyl][2-(2-phenyl-1,1,1-trifluoroethyl)]hydroxylamine

Guidance literature:

With hydrogenchloride; In tetrahydrofuran; water; at 20 ℃; for 24h;

DOI:10.1021/jo000685l

upstream raw materials:

N-benzyl-4-(trifluoromethyl)aniline

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