((3R,4R)-4-Hydroxymethyl-tetrahydro-furan-3-yl)-carbamic acid benzyl ester

Base Information

• Chemical Name: ((3R,4R)-4-Hydroxymethyl-tetrahydro-furan-3-yl)-carbamic acid benzyl ester
• CAS No.: 623582-55-8
• Molecular Formula: C₁₃H₁₇NO₄
• Molecular Weight: 251.282

Synonyms:((3R,4R)-4-Hydroxymethyl-tetrahydro-furan-3-yl)-carbamic acid benzyl ester

Chemical Property of ((3R,4R)-4-Hydroxymethyl-tetrahydro-furan-3-yl)-carbamic acid benzyl ester

Chemical Property:

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Technology Process of ((3R,4R)-4-Hydroxymethyl-tetrahydro-furan-3-yl)-carbamic acid benzyl ester

There total 3 articles about ((3R,4R)-4-Hydroxymethyl-tetrahydro-furan-3-yl)-carbamic acid benzyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

2-(allyloxy)acetaldehyde (55207-76-6) → ((3R,4R)-4-Hydroxymethyl-tetrahydro-furan-3-yl)-carbamic acid benzyl ester (623582-55-8)

Guidance literature:

Multi-step reaction with 3 steps

1: 89 percent / MgBr₂; 2-propanol / CH₂Cl₂ / 1 h / 40 °C

2: H₂ / Pd(OH)2/C / methanol / 760 Torr

3: 350 mg / NaHCO₃ / tetrahydrofuran; H₂O / 20 °C

With hydrogen; sodium hydrogencarbonate; isopropyl alcohol; magnesium bromide; palladium dihydroxide; In tetrahydrofuran; methanol; dichloromethane; water;

DOI:10.1021/jo034940o

Reference yield:

(R)-2-Phenyl-2-(3aS,6aR)-tetrahydro-furo[3,4-c]isoxazol-1-yl-ethanol (623582-46-7) → ((3R,4R)-4-Hydroxymethyl-tetrahydro-furan-3-yl)-carbamic acid benzyl ester (623582-55-8)

Guidance literature:

Multi-step reaction with 2 steps

1: H₂ / Pd(OH)2/C / methanol / 760 Torr

2: 350 mg / NaHCO₃ / tetrahydrofuran; H₂O / 20 °C

With hydrogen; sodium hydrogencarbonate; palladium dihydroxide; In tetrahydrofuran; methanol; water;

DOI:10.1021/jo034940o

Reference yield:

benzyl chloroformate (501-53-1,94274-21-2) + ((3R,4R)-4-Amino-tetrahydro-furan-3-yl)-methanol → ((3R,4R)-4-Hydroxymethyl-tetrahydro-furan-3-yl)-carbamic acid benzyl ester (623582-55-8)

Guidance literature:

With sodium hydrogencarbonate; In tetrahydrofuran; water; at 20 ℃;

DOI:10.1021/jo034940o

upstream raw materials:

benzyl chloroformate

2-(allyloxy)acetaldehyde

(R)-2-Phenyl-2-(3aS,6aR)-tetrahydro-furo[3,4-c]isoxazol-1-yl-ethanol

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