3,12-bis(dicyanomethylene)-2,13-bis[4-(dihexylamino)phenyl]-1,13-tetradecadiene-4,6,8,10-tetrayne-1,1,14,14-tetracarbonitrile

Base Information

• Chemical Name: 3,12-bis(dicyanomethylene)-2,13-bis[4-(dihexylamino)phenyl]-1,13-tetradecadiene-4,6,8,10-tetrayne-1,1,14,14-tetracarbonitrile
• CAS No.: 1229035-62-4
• Molecular Formula: C₆₀H₆₀N₁₀
• Molecular Weight: 921.203

Synonyms:3,12-bis(dicyanomethylene)-2,13-bis[4-(dihexylamino)phenyl]-1,13-tetradecadiene-4,6,8,10-tetrayne-1,1,14,14-tetracarbonitrile

Chemical Property of 3,12-bis(dicyanomethylene)-2,13-bis[4-(dihexylamino)phenyl]-1,13-tetradecadiene-4,6,8,10-tetrayne-1,1,14,14-tetracarbonitrile

Chemical Property:

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Technology Process of 3,12-bis(dicyanomethylene)-2,13-bis[4-(dihexylamino)phenyl]-1,13-tetradecadiene-4,6,8,10-tetrayne-1,1,14,14-tetracarbonitrile

There total 2 articles about 3,12-bis(dicyanomethylene)-2,13-bis[4-(dihexylamino)phenyl]-1,13-tetradecadiene-4,6,8,10-tetrayne-1,1,14,14-tetracarbonitrile which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

4,4'-(dodeca-1,3,5,7,9,11-hexayne-1,12-diyl)bis(N,N-dihexylaniline) (1229035-53-3) + ethenetetracarbonitrile (670-54-2) → 3,12-bis(dicyanomethylene)-2,13-bis[4-(dihexylamino)phenyl]-1,13-tetradecadiene-4,6,8,10-tetrayne-1,1,14,14-tetracarbonitrile (1229035-62-4)

Guidance literature:

In dichloromethane; at 25 ℃; for 18h; Inert atmosphere;

DOI:10.1002/ejoc.201000030

Reference yield: 39.0%

4,4'-(dodeca-1,3,5,7,9,11-hexayne-1,12-diyl)bis(N,N-dihexylaniline) (1229035-53-3) + ethenetetracarbonitrile (670-54-2) → 2-[4-(dihexylamino)phenyl]-3-{10-[4-(dihexylamino)phenyl]-1,3,5,7,9-decapentayn-1-yl}-1,3-butadiene-1,1,4,4-tetracarbonitrile (1229035-61-3) + 3,12-bis(dicyanomethylene)-2,13-bis[4-(dihexylamino)phenyl]-1,13-tetradecadiene-4,6,8,10-tetrayne-1,1,14,14-tetracarbonitrile (1229035-62-4)

Guidance literature:

In dichloromethane; at 25 ℃; for 3h; Inert atmosphere;

DOI:10.1002/ejoc.201000030

Reference yield: 58.0%

tetrathiafulvalene (31366-25-3) + 3,12-bis(dicyanomethylene)-2,13-bis[4-(dihexylamino)phenyl]-1,13-tetradecadiene-4,6,8,10-tetrayne-1,1,14,14-tetracarbonitrile (1229035-62-4) → 3,12-bis(dicyanomethylene)-2,13-bis[4-(dihexylamino)phenyl]-4,5,10,11-tetra(1,3-dithiol-2-ylidene)-1,13-tetradecadiene-6,8-diyne-1,1,14,14-tetracarbonitrile (1229035-63-5)

Guidance literature:

In dichloromethane; acetonitrile; at 50 ℃; for 6h; Inert atmosphere;

DOI:10.1002/ejoc.201000030

upstream raw materials:

4,4'-(dodeca-1,3,5,7,9,11-hexayne-1,12-diyl)bis(N,N-dihexylaniline)

ethenetetracarbonitrile

Downstream raw materials:

3,12-bis(dicyanomethylene)-2,13-bis[4-(dihexylamino)phenyl]-4,5,10,11-tetra(1,3-dithiol-2-ylidene)-1,13-tetradecadiene-6,8-diyne-1,1,14,14-tetracarbonitrile

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