C₃₀H₂₆BF₂N₃

Base Information

• Chemical Name: C₃₀H₂₆BF₂N₃
• CAS No.: 1607827-58-6
• Molecular Formula: C₃₀H₂₆BF₂N₃
• Molecular Weight: 477.364
• Mol file: 1607827-58-6.mol

Synonyms:C₃₀H₂₆BF₂N₃

Chemical Property of C₃₀H₂₆BF₂N₃

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₃₀H₂₆BF₂N₃

There total 6 articles about C₃₀H₂₆BF₂N₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

C43H34BF2N3 (1607827-57-5) → C30H26BF2N3 (1607827-58-6)

Guidance literature:

With hydrogenchloride; In tetrahydrofuran; water; at 70 ℃; for 1h;

DOI:10.1021/ol501131j

Reference yield:

2-phenyl-1H-pyrrole (3042-22-6) → C30H26BF2N3 (1607827-58-6)

Guidance literature:

Multi-step reaction with 6 steps

1: trifluoroacetic acid / dichloromethane / 3 h / 20 °C / Inert atmosphere

2: 2,3-dicyano-5,6-dichloro-p-benzoquinone / dichloromethane / 2 h / 20 °C

3: N-ethyl-N,N-diisopropylamine / dichloromethane / 6 h / 0 - 20 °C / Inert atmosphere

4: N-Bromosuccinimide; 2,2'-azobis(isobutyronitrile) / dichloromethane; methanol / 25 h / 100 °C / Inert atmosphere

5: caesium carbonate; tris(dibenzylideneacetone)dipalladium⁽⁰⁾ chloroform complex; 4,5-bis(diphenylphosphino)-9,9-dimethylxanthene / 1,4-dioxane / 15 h / 100 °C / Inert atmosphere; Schlenk technique

6: hydrogenchloride / tetrahydrofuran; water / 1 h / 70 °C

With hydrogenchloride; tris(dibenzylideneacetone)dipalladium⁽⁰⁾ chloroform complex; N-Bromosuccinimide; 2,2'-azobis(isobutyronitrile); caesium carbonate; N-ethyl-N,N-diisopropylamine; 4,5-bis(diphenylphosphino)-9,9-dimethylxanthene; trifluoroacetic acid; 2,3-dicyano-5,6-dichloro-p-benzoquinone; In tetrahydrofuran; 1,4-dioxane; methanol; dichloromethane; water;

DOI:10.1021/ol501131j

Reference yield:

3,8-diphenyl-5-mesityldipyrromethane (1607823-19-7) → C30H26BF2N3 (1607827-58-6)

Guidance literature:

Multi-step reaction with 5 steps

1: 2,3-dicyano-5,6-dichloro-p-benzoquinone / dichloromethane / 2 h / 20 °C

2: N-ethyl-N,N-diisopropylamine / dichloromethane / 6 h / 0 - 20 °C / Inert atmosphere

3: N-Bromosuccinimide; 2,2'-azobis(isobutyronitrile) / dichloromethane; methanol / 25 h / 100 °C / Inert atmosphere

4: caesium carbonate; tris(dibenzylideneacetone)dipalladium⁽⁰⁾ chloroform complex; 4,5-bis(diphenylphos4,5-bis(diphenylphosphino)-9,9-dimethylxanthenephino)-9,9-dimethylxanthene / 1,4-dioxane / 15 h / 100 °C / Inert atmosphere; Schlenk technique

5: hydrogenchloride / tetrahydrofuran; water / 1 h / 70 °C

With hydrogenchloride; tris(dibenzylideneacetone)dipalladium⁽⁰⁾ chloroform complex; N-Bromosuccinimide; 2,2'-azobis(isobutyronitrile); caesium carbonate; N-ethyl-N,N-diisopropylamine; 4,5-bis(diphenylphos4,5-bis(diphenylphosphino)-9,9-dimethylxanthenephino)-9,9-dimethylxanthene; 2,3-dicyano-5,6-dichloro-p-benzoquinone; In tetrahydrofuran; 1,4-dioxane; methanol; dichloromethane; water;

DOI:10.1021/ol501131j

upstream raw materials:

C₃₀H₂₄BBrF₂N₂

C₄₃H₃₄BF₂N₃

2-phenyl-1H-pyrrole

3,8-diphenyl-5-mesityldipyrromethane

Downstream raw materials:

C₆₀H₄₈B₂F₄N₆

C₆₀H₄₉B₂F₄N₇