(E/Z)-N-(2-nitrobenzylidene)-2,4,6-trichlorophenylsulfenamide

Base Information

• Chemical Name: (E/Z)-N-(2-nitrobenzylidene)-2,4,6-trichlorophenylsulfenamide
• CAS No.: 321657-80-1
• Molecular Formula: C₁₃H₇Cl₃N₂O₂S
• Molecular Weight: 361.636
• Mol file: 321657-80-1.mol

Synonyms:(E/Z)-N-(2-nitrobenzylidene)-2,4,6-trichlorophenylsulfenamide

Chemical Property of (E/Z)-N-(2-nitrobenzylidene)-2,4,6-trichlorophenylsulfenamide

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
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MSDS Files:

Useful:

Technology Process of (E/Z)-N-(2-nitrobenzylidene)-2,4,6-trichlorophenylsulfenamide

There total 1 articles about (E/Z)-N-(2-nitrobenzylidene)-2,4,6-trichlorophenylsulfenamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 65.0%

2,4,6-trichlorosulfenamide (17162-41-3) + 2-nitro-benzaldehyde (552-89-6) → (E/Z)-N-(2-nitrobenzylidene)-2,4,6-trichlorophenylsulfenamide (321657-80-1)

Guidance literature:

With tetraethoxy orthosilicate; toluene-4-sulfonic acid; In toluene; Heating;

DOI:10.1007/BF02297680

Reference yield:

(E/Z)-N-(2-nitrobenzylidene)-2,4,6-trichlorophenylsulfenamide (321657-80-1) → C13H9Cl3N2S

Guidance literature:

With hydrogen; palladium on activated charcoal; In ethanol; for 2.5h; under 1034.3 Torr;

DOI:10.1007/BF02297680

Reference yield:

(E/Z)-N-(2-nitrobenzylidene)-2,4,6-trichlorophenylsulfenamide (321657-80-1) → C16H13Cl3N2OS

Guidance literature:

Multi-step reaction with 2 steps

1: H₂ / Pd/C / ethanol / 2.5 h / 1034.3 Torr

2: Heating

With hydrogen; palladium on activated charcoal; In ethanol;

DOI:10.1007/BF02297680

upstream raw materials:

2,4,6-trichlorosulfenamide

2-nitro-benzaldehyde