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2,4-Dichloro-benzoic acid 4-methoxy-5-methylene-2-oxo-2,5-dihydro-furan-3-yl ester

Base Information Edit
  • Chemical Name:2,4-Dichloro-benzoic acid 4-methoxy-5-methylene-2-oxo-2,5-dihydro-furan-3-yl ester
  • CAS No.:125011-17-8
  • Molecular Formula:C13H8Cl2O5
  • Molecular Weight:315.11
  • Hs Code.:
  • Mol file:125011-17-8.mol
2,4-Dichloro-benzoic acid 4-methoxy-5-methylene-2-oxo-2,5-dihydro-furan-3-yl ester

Synonyms:2,4-Dichloro-benzoic acid 4-methoxy-5-methylene-2-oxo-2,5-dihydro-furan-3-yl ester

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The product has achieved commercial mass production*data from LookChem market partment
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Chemical Property of 2,4-Dichloro-benzoic acid 4-methoxy-5-methylene-2-oxo-2,5-dihydro-furan-3-yl ester Edit
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Technology Process of 2,4-Dichloro-benzoic acid 4-methoxy-5-methylene-2-oxo-2,5-dihydro-furan-3-yl ester

There total 2 articles about 2,4-Dichloro-benzoic acid 4-methoxy-5-methylene-2-oxo-2,5-dihydro-furan-3-yl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:
Guidance literature:
With triethylamine; dicyclohexyl-carbodiimide; In dichloromethane; Ambient temperature;
DOI:10.1016/S0040-4039(00)99656-4
Guidance literature:
Multi-step reaction with 2 steps
1: 1) LiN(i-Pr)2; 2) B(OMe)3, H2O2 / 1) THF, -90 deg C
2: 83 percent / Et3N, N,N'-dicyclohexylcarbodiimide / CH2Cl2 / Ambient temperature
With Trimethyl borate; dihydrogen peroxide; triethylamine; dicyclohexyl-carbodiimide; lithium diisopropyl amide; In dichloromethane;
DOI:10.1016/S0040-4039(00)99656-4
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