C₂₅H₂₇NO

Base Information

Chemical Name:C₂₅H₂₇NO
CAS No.:1588489-02-4
Molecular Formula:C₂₅H₂₇NO
Molecular Weight:357.495
Hs Code.:

Synonyms:C₂₅H₂₇NO

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Chemical Property of C₂₅H₂₇NO

Chemical Property:

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Technology Process of C₂₅H₂₇NO

There total 7 articles about C₂₅H₂₇NO which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 25.0%

: 1588488-85-0
C₂₅H₂₈NO⁽¹⁺⁾*CF₃O₃S^(1-)

: 1588489-02-4
C₂₅H₂₇NO

Guidance literature:: With potassium tert-butylate; In tetrahydrofuran; at 0 - 20 ℃; for 2h; regioselective reaction; Inert atmosphere;
DOI:10.1002/ejoc.201301536 DOI:10.1002/ejoc.201301536

Reference yield:

: 18809-63-7
2-diphenylmethylamino-ethanol

: 1588489-02-4
C₂₅H₂₇NO

Guidance literature:: Multi-step reaction with 8 steps

1.1: potassium carbonate; sodium iodide / dichloromethane / 16 h / Reflux; Inert atmosphere

2.1: thionyl chloride / dichloromethane / 2 h / 20 °C / Inert atmosphere

3.1: potassium tert-butylate / tetrahydrofuran / 16 h / 20 °C / Inert atmosphere

4.1: sulfuric acid / 144 h / 60 °C / Inert atmosphere

5.1: lithium aluminium tetrahydride / tetrahydrofuran / 0 - 50 °C / Inert atmosphere

6.1: sodium hydride / N,N-dimethyl-formamide; mineral oil / 0.33 h / 0 °C / Inert atmosphere

6.2: 12.5 h / 20 - 60 °C / Inert atmosphere

6.3: 5 h / 60 °C / Inert atmosphere

7.1: dichloromethane / 3 h / 0 - 20 °C / Inert atmosphere

8.1: potassium tert-butylate / tetrahydrofuran / 2 h / 0 - 20 °C / Inert atmosphere

With lithium aluminium tetrahydride; thionyl chloride; sulfuric acid; potassium tert-butylate; sodium hydride; potassium carbonate; sodium iodide; In tetrahydrofuran; dichloromethane; N,N-dimethyl-formamide; mineral oil; 8.1: |Stevens Rearrangement;
DOI:10.1002/ejoc.201301536

Reference yield:

: 71556-64-4
N-Benzhydryl-2-carbethoxyazetidine

: 1588489-02-4
C₂₅H₂₇NO

Guidance literature:: Multi-step reaction with 4 steps

1.1: lithium aluminium tetrahydride / tetrahydrofuran / 0 - 50 °C / Inert atmosphere

2.1: sodium hydride / N,N-dimethyl-formamide; mineral oil / 0.33 h / 0 °C / Inert atmosphere

2.2: 12.5 h / 20 - 60 °C / Inert atmosphere

2.3: 5 h / 60 °C / Inert atmosphere

3.1: dichloromethane / 3 h / 0 - 20 °C / Inert atmosphere

4.1: potassium tert-butylate / tetrahydrofuran / 2 h / 0 - 20 °C / Inert atmosphere

With lithium aluminium tetrahydride; potassium tert-butylate; sodium hydride; In tetrahydrofuran; dichloromethane; N,N-dimethyl-formamide; mineral oil; 4.1: |Stevens Rearrangement;
DOI:10.1002/ejoc.201301536