di-O-acetyl-1,2-O-benzoyl-5-desoxy-3-trifluoroacetamido-3-α et β-D-ribofurannoses

Base Information

Chemical Name:di-O-acetyl-1,2-O-benzoyl-5-desoxy-3-trifluoroacetamido-3-α et β-D-ribofurannoses
CAS No.:91384-34-8
Molecular Formula:C₁₈H₁₈F₃NO₈
Molecular Weight:433.338
Hs Code.:

Synonyms:di-O-acetyl-1,2-O-benzoyl-5-desoxy-3-trifluoroacetamido-3-α et β-D-ribofurannoses

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Chemical Property of di-O-acetyl-1,2-O-benzoyl-5-desoxy-3-trifluoroacetamido-3-α et β-D-ribofurannoses

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Technology Process of di-O-acetyl-1,2-O-benzoyl-5-desoxy-3-trifluoroacetamido-3-α et β-D-ribofurannoses

There total 3 articles about di-O-acetyl-1,2-O-benzoyl-5-desoxy-3-trifluoroacetamido-3-α et β-D-ribofurannoses which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 67.0%

: 70894-62-1
3-(trifluoroacetamido)-1,2-O-isopropylidene-5-O-benzoyl-3-deoxy-α-D-ribofuranose

: 108-24-7
acetic anhydride

: 91384-34-8
di-O-acetyl-1,2-O-benzoyl-5-desoxy-3-trifluoroacetamido-3-α et β-D-ribofurannoses

Guidance literature:: With sulfuric acid; In acetic acid; at 20 ℃; for 14h;
DOI:10.1002/hlca.19800630814

Reference yield:

: 29781-49-5
desoxy-3-O-isopropylidene-1,2-trifluoroacetamido-3-α-D-ribofurannose

: 91384-34-8
di-O-acetyl-1,2-O-benzoyl-5-desoxy-3-trifluoroacetamido-3-α et β-D-ribofurannoses

Guidance literature:: Multi-step reaction with 2 steps

1: 80 percent / pyridine / 14 h / 4 °C

2: 67 percent / H₂SO₄ / acetic acid / 14 h / 20 °C

With sulfuric acid; In pyridine; acetic acid;
DOI:10.1002/hlca.19800630814

Reference yield:

: 78188-23-5
3-O-isopropylidene-1,2-trifluoroacetamido-3-α-D-ribopentodialdofurannose

: 91384-34-8
di-O-acetyl-1,2-O-benzoyl-5-desoxy-3-trifluoroacetamido-3-α et β-D-ribofurannoses

Guidance literature:: Multi-step reaction with 3 steps

1: 73 percent / NaBH₄ / acetic acid / 2 h / 0 °C

2: 80 percent / pyridine / 14 h / 4 °C

3: 67 percent / H₂SO₄ / acetic acid / 14 h / 20 °C

With sodium tetrahydroborate; sulfuric acid; In pyridine; acetic acid;
DOI:10.1002/hlca.19800630814