1-(3-(2-(1-benzyl-1H-tetrazol-5-yl)ethyl)-4,6,7-trifluoro-2,3-dihydropyrrolo[3,2-c]pyridin-1-yl)ethanone

Base Information

Chemical Name:1-(3-(2-(1-benzyl-1H-tetrazol-5-yl)ethyl)-4,6,7-trifluoro-2,3-dihydropyrrolo[3,2-c]pyridin-1-yl)ethanone
CAS No.:1239316-88-1
Molecular Formula:C₁₉H₁₇F₃N₆O
Molecular Weight:402.379
Hs Code.:

Synonyms:1-(3-(2-(1-benzyl-1H-tetrazol-5-yl)ethyl)-4,6,7-trifluoro-2,3-dihydropyrrolo[3,2-c]pyridin-1-yl)ethanone

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Chemical Property of 1-(3-(2-(1-benzyl-1H-tetrazol-5-yl)ethyl)-4,6,7-trifluoro-2,3-dihydropyrrolo[3,2-c]pyridin-1-yl)ethanone

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Technology Process of 1-(3-(2-(1-benzyl-1H-tetrazol-5-yl)ethyl)-4,6,7-trifluoro-2,3-dihydropyrrolo[3,2-c]pyridin-1-yl)ethanone

There total 2 articles about 1-(3-(2-(1-benzyl-1H-tetrazol-5-yl)ethyl)-4,6,7-trifluoro-2,3-dihydropyrrolo[3,2-c]pyridin-1-yl)ethanone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 27.0%

: 1239316-86-9
S-4-(1-benzyl-1H-tetrazol-5-yl)-1-(N-(perfluoropyridin-4-yl)acetamido)butan-2-yl O-ethyl carbonodithioate

: 1239316-88-1
1-(3-(2-(1-benzyl-1H-tetrazol-5-yl)ethyl)-4,6,7-trifluoro-2,3-dihydropyrrolo[3,2-c]pyridin-1-yl)ethanone

Guidance literature:: With di-tert-butyl peroxide; In 1,2-dichloro-benzene; for 2.5h; Inert atmosphere; Reflux;
DOI:10.1021/ol101240f

Reference yield:

: 1239316-68-7
N-allyl-N-(perfluoropyridin-4-yl)acetamide

: 201672-89-1
Dithiocarbonic acid S-(1-benzyl-1H-tetrazol-5-ylmethyl) ester O-ethyl ester

: 1239316-88-1
1-(3-(2-(1-benzyl-1H-tetrazol-5-yl)ethyl)-4,6,7-trifluoro-2,3-dihydropyrrolo[3,2-c]pyridin-1-yl)ethanone

Guidance literature:: Multi-step reaction with 2 steps

1: dilauryl peroxide / ethyl acetate / Reflux; Inert atmosphere

2: di-tert-butyl peroxide / 1,2-dichloro-benzene / Reflux; Inert atmosphere

With di-tert-butyl peroxide; dilauryl peroxide; In ethyl acetate; 1,2-dichloro-benzene;
DOI:10.1071/CH10422