C₁₄H₂₀Br₂O

Base Information

• Chemical Name: C₁₄H₂₀Br₂O
• CAS No.: 1240047-14-6
• Molecular Formula: C₁₄H₂₀Br₂O
• Molecular Weight: 364.12
• Mol file: 1240047-14-6.mol

Synonyms:C₁₄H₂₀Br₂O

Chemical Property of C₁₄H₂₀Br₂O

Chemical Property:

Purity/Quality:

99% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₁₄H₂₀Br₂O

There total 1 articles about C₁₄H₂₀Br₂O which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

1-bromo-octane (111-83-1) + 3,5-dibromophenol (626-41-5) → C14H20Br2O (1240047-14-6)

Guidance literature:

With potassium carbonate; In N,N-dimethyl-formamide; at 100 ℃; for 24h; Inert atmosphere; Schlenk technique;

DOI:10.1021/jacs.0c00110

Reference yield: 70.0%

4′-(4-boronatophenyl)-2,2′:6′,2′′-terpyridine (381218-96-8) + C14H20Br2O (1240047-14-6) → C56H48N6O

Guidance literature:

With bis-triphenylphosphine-palladium(II) chloride; sodium carbonate; In water; toluene; tert-butyl alcohol; at 85 ℃; for 48h; Inert atmosphere; Schlenk technique;

DOI:10.1021/jacs.0c00110

Reference yield: 64.0%

4,4'-dibromo-2,2'-bipyridine (18511-71-2) + C14H20Br2O (1240047-14-6) → C38H46Br2N2O2 (1256573-50-8)

Guidance literature:

C₁₄H₂₀Br₂O; With n-butyllithium; In tetrahydrofuran; hexane; at -78 ℃; for 1h; Inert atmosphere;

4,4'-dibromo-2,2'-bipyridine; With tetrakis(triphenylphosphine) palladium⁽⁰⁾; zinc(II) chloride; In tetrahydrofuran; hexane; at 0 - 20 ℃; Inert atmosphere;

DOI:10.1021/ja106599j

upstream raw materials:

1-bromo-octane

3,5-dibromophenol

Downstream raw materials:

C₃₈H₄₆Br₂N₂O₂