piperidine-1-carbodithioic acid 2-nitrophenyl ester

Base Information

Chemical Name:piperidine-1-carbodithioic acid 2-nitrophenyl ester
CAS No.:10363-70-9
Molecular Formula:C₁₂H₁₄N₂O₂S₂
Molecular Weight:282.387
Hs Code.:

Synonyms:piperidine-1-carbodithioic acid 2-nitrophenyl ester

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of piperidine-1-carbodithioic acid 2-nitrophenyl ester

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Technology Process of piperidine-1-carbodithioic acid 2-nitrophenyl ester

There total 4 articles about piperidine-1-carbodithioic acid 2-nitrophenyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

: 110-89-4
piperidine

: 75-15-0,12122-00-8
carbon disulfide

: 88-74-4
2-nitro-aniline

: 10363-70-9
piperidine-1-carbodithioic acid 2-nitrophenyl ester

Guidance literature:: 2-nitro-aniline; With sodium nitrite; In water; at 20 ℃; for 0.166667h; Milling; Green chemistry;

piperidine; carbon disulfide; In water; at 20 ℃; for 0.283333h; Green chemistry;
DOI:10.1080/10426507.2015.1024311

Reference yield:

: 98-99-7
piperidine-1-carbodithioic acid

: 365-33-3
2-nitrobenzenediazonium tetrafluoroborate

: 10363-70-9
piperidine-1-carbodithioic acid 2-nitrophenyl ester

Guidance literature:: In water; at 25 ℃; for 2.5h;
DOI:10.1039/c1gc00001b

Reference yield:

: 110-89-4
piperidine

: 10363-70-9
piperidine-1-carbodithioic acid 2-nitrophenyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: water / 0.08 h / 0 - 5 °C

2: water / 2.5 h / 25 °C

In water;
DOI:10.1039/c1gc00001b