Technology Process of C24H26FN3O2S
There total 5 articles about C24H26FN3O2S which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
Multi-step reaction with 2 steps
1.1: acetic anhydride; triethylamine / 15 h / 145 °C
2.1: triethylamine; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / dichloromethane / 0.08 h / 23 °C
2.2: 15 h
With
acetic anhydride; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine;
In
dichloromethane;
DOI:10.1021/jm300833h
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: sodium acetate / water / 24 h / 90 °C / Inert atmosphere
2.1: iron; acetic acid / 2.5 h / 80 - 92 °C / Inert atmosphere
3.1: acetic anhydride; triethylamine / 15 h / 145 °C
4.1: triethylamine; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / dichloromethane / 0.08 h / 23 °C
4.2: 15 h
With
sodium acetate; acetic anhydride; iron; benzotriazol-1-ol; acetic acid; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine;
In
dichloromethane; water;
DOI:10.1021/jm300833h
- Guidance literature:
-
Multi-step reaction with 2 steps
1.1: dichloromethane / 4 h / 0 - 23 °C
2.1: triethylamine; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / dichloromethane / 0.08 h / 23 °C
2.2: 15 h
With
benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine;
In
dichloromethane;
DOI:10.1021/jm300833h