3-cyclohexylimino-2-(diisopropoxy-phosphoryloxy)-acrylic acid ethyl ester

Base Information

• Chemical Name: 3-cyclohexylimino-2-(diisopropoxy-phosphoryloxy)-acrylic acid ethyl ester
• CAS No.: 1146344-31-1
• Molecular Formula: C₁₇H₃₀NO₆P
• Molecular Weight: 375.402

Synonyms:3-cyclohexylimino-2-(diisopropoxy-phosphoryloxy)-acrylic acid ethyl ester

Chemical Property of 3-cyclohexylimino-2-(diisopropoxy-phosphoryloxy)-acrylic acid ethyl ester

Chemical Property:

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Technology Process of 3-cyclohexylimino-2-(diisopropoxy-phosphoryloxy)-acrylic acid ethyl ester

There total 2 articles about 3-cyclohexylimino-2-(diisopropoxy-phosphoryloxy)-acrylic acid ethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

triisopropyl phosphite (116-17-6) + ethyl 3-chloro-3-(cyclohexylimino)-2-oxopropanoate → 3-cyclohexylimino-2-(diisopropoxy-phosphoryloxy)-acrylic acid ethyl ester (1146344-31-1)

Guidance literature:

at 20 ℃; for 0.0833333h; Inert atmosphere;

DOI:10.1021/ol9004432

Reference yield:

Cyclohexyl isocyanide (931-53-3) → 3-cyclohexylimino-2-(diisopropoxy-phosphoryloxy)-acrylic acid ethyl ester (1146344-31-1)

Guidance literature:

Multi-step reaction with 2 steps

1: acetonitrile / 0.17 h / 20 °C

2: acetonitrile / 0.08 h / 20 °C

In acetonitrile;

DOI:10.1016/j.tet.2013.01.023

Reference yield: 79.0%

3-cyclohexylimino-2-(diisopropoxy-phosphoryloxy)-acrylic acid ethyl ester (1146344-31-1) + diazomethyl-trimethyl-silane (18107-18-1) → (3-cyclohexyl-3H-[1,2,3]triazol-4-yl)-(diisopropoxy-phosphoryloxy)-acetic acid ethyl ester (1146344-45-7)

Guidance literature:

In hexane; tert-butyl alcohol; at 20 ℃;

DOI:10.1021/ol9004432

upstream raw materials:

triisopropyl phosphite

Cyclohexyl isocyanide

Downstream raw materials:

(3-cyclohexyl-3H-[1,2,3]triazol-4-yl)-(diisopropoxy-phosphoryloxy)-acetic acid ethyl ester

C₁₉H₂₄N₂O₄

C₂₄H₂₅BrN₂O₃

C₂₆H₂₇ClN₂O₂

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