4′-[(2,3-dihydro-1H-inden-2-ylamino)methyl]-3-biphenylcarboxamide trifluoroacetate

Base Information

Chemical Name:4′-[(2,3-dihydro-1H-inden-2-ylamino)methyl]-3-biphenylcarboxamide trifluoroacetate
CAS No.:1007575-91-8
Molecular Formula:C₂HF₃O₂*C₂₃H₂₂N₂O
Molecular Weight:456.464
Hs Code.:

Synonyms:4′-[(2,3-dihydro-1H-inden-2-ylamino)methyl]-3-biphenylcarboxamide trifluoroacetate

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Chemical Property of 4′-[(2,3-dihydro-1H-inden-2-ylamino)methyl]-3-biphenylcarboxamide trifluoroacetate

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Technology Process of 4′-[(2,3-dihydro-1H-inden-2-ylamino)methyl]-3-biphenylcarboxamide trifluoroacetate

There total 4 articles about 4′-[(2,3-dihydro-1H-inden-2-ylamino)methyl]-3-biphenylcarboxamide trifluoroacetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1007579-69-2
4′-formyl-3-biphenylcarboxamide

: 2975-41-9
2,3-dihydro-1H-inden-2-amine

: 76-05-1
trifluoroacetic acid

: 1007575-91-8
4′-[(2,3-dihydro-1H-inden-2-ylamino)methyl]-3-biphenylcarboxamide trifluoroacetate

Guidance literature:: 4′-formyl-3-biphenylcarboxamide; 2,3-dihydro-1H-inden-2-amine; With acetic acid; In methanol; dichloromethane; at 20 ℃; for 0.5h;

trifluoroacetic acid; In water; acetonitrile;

Reference yield:

: 1007579-69-2
4′-formyl-3-biphenylcarboxamide

: PS-BH₃CN

: 2975-41-9
2,3-dihydro-1H-inden-2-amine

: 1007575-91-8
4′-[(2,3-dihydro-1H-inden-2-ylamino)methyl]-3-biphenylcarboxamide trifluoroacetate

Guidance literature:: With acetic acid; trifluoroacetic acid; In methanol; CH₂Cl₂/HOAc; dichloromethane;

Reference yield:

: 351422-73-6
(3-(aminocarbonyl)phenyl)boronic acid

: 1007575-91-8
4′-[(2,3-dihydro-1H-inden-2-ylamino)methyl]-3-biphenylcarboxamide trifluoroacetate

Guidance literature:: Multi-step reaction with 2 steps

1: sodium carbonate; dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH₂Cl₂ / 1,2-dimethoxyethane / 1.83 h / Inert atmosphere

2: acetic acid / methanol; dichloromethane / 0.5 h / 20 °C

With dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH₂Cl₂; sodium carbonate; acetic acid; In methanol; 1,2-dimethoxyethane; dichloromethane; 1: |Suzuki Coupling;