benzyl (S)-2-(tert-butyloxycarbonylamino)-3-oxopent-4-enyl sulfide

Base Information

Chemical Name:benzyl (S)-2-(tert-butyloxycarbonylamino)-3-oxopent-4-enyl sulfide
CAS No.:934476-24-1
Molecular Formula:C₁₇H₂₃NO₃S
Molecular Weight:321.441
Hs Code.:

Synonyms:benzyl (S)-2-(tert-butyloxycarbonylamino)-3-oxopent-4-enyl sulfide

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Chemical Property of benzyl (S)-2-(tert-butyloxycarbonylamino)-3-oxopent-4-enyl sulfide

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Technology Process of benzyl (S)-2-(tert-butyloxycarbonylamino)-3-oxopent-4-enyl sulfide

There total 1 articles about benzyl (S)-2-(tert-butyloxycarbonylamino)-3-oxopent-4-enyl sulfide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 593-60-2,25951-54-6
Vinyl bromide

: 208521-21-5
S-Benzyl-N_α-(tert-butyloxycarbonyl)-cysteine-N-methoxy-N-methylamide

: 934476-24-1
benzyl (S)-2-(tert-butyloxycarbonylamino)-3-oxopent-4-enyl sulfide

Guidance literature:: Vinyl bromide; With magnesium; In tetrahydrofuran; Reflux;

S-Benzyl-N_α-(tert-butyloxycarbonyl)-cysteine-N-methoxy-N-methylamide; In tetrahydrofuran; at 20 ℃; for 0.166667h;

With hydrogenchloride; In tetrahydrofuran; water; at 0 ℃;
DOI:10.1016/j.tet.2008.10.018

Reference yield: 98.0%

: 934476-24-1
benzyl (S)-2-(tert-butyloxycarbonylamino)-3-oxopent-4-enyl sulfide

: 934476-25-2
(2S,3R)-1-benzylthio-2-(tert-butyloxycarbonylamino)pent-4-en-3-ol

Guidance literature:: With lithium tri-t-butoxyaluminum hydride; In tetrahydrofuran; ethanol; at -78 ℃; for 0.25h;
DOI:10.1016/j.tet.2008.10.018