2-[N-(tert-butyloxycarbonyl)-N-(3-chloroprop-2-en-1-yl)-amino]-4-benzyloxy-1,9-dibromoanthracene

Base Information

Chemical Name:2-[N-(tert-butyloxycarbonyl)-N-(3-chloroprop-2-en-1-yl)-amino]-4-benzyloxy-1,9-dibromoanthracene
CAS No.:1187567-03-8
Molecular Formula:C₂₉H₂₆Br₂ClNO₃
Molecular Weight:631.791
Hs Code.:

Synonyms:2-[N-(tert-butyloxycarbonyl)-N-(3-chloroprop-2-en-1-yl)-amino]-4-benzyloxy-1,9-dibromoanthracene

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Chemical Property of 2-[N-(tert-butyloxycarbonyl)-N-(3-chloroprop-2-en-1-yl)-amino]-4-benzyloxy-1,9-dibromoanthracene

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Technology Process of 2-[N-(tert-butyloxycarbonyl)-N-(3-chloroprop-2-en-1-yl)-amino]-4-benzyloxy-1,9-dibromoanthracene

There total 1 articles about 2-[N-(tert-butyloxycarbonyl)-N-(3-chloroprop-2-en-1-yl)-amino]-4-benzyloxy-1,9-dibromoanthracene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

: 542-75-6
E/Z-1,3-Dichloropropene

: 1187567-02-7
4-benzyloxy-2-(tert-butyloxycarbonyl)amino-1,9-dibromoanthracene

: 1187567-03-8
2-[N-(tert-butyloxycarbonyl)-N-(3-chloroprop-2-en-1-yl)-amino]-4-benzyloxy-1,9-dibromoanthracene

Guidance literature:: 4-benzyloxy-2-(tert-butyloxycarbonyl)amino-1,9-dibromoanthracene; With tetra-(n-butyl)ammonium iodide; sodium hydride; In N,N-dimethyl-formamide; mineral oil; at 0 ℃; for 0.5h; Inert atmosphere;

E/Z-1,3-Dichloropropene; In N,N-dimethyl-formamide; mineral oil; at 0 ℃; for 2h; Darkness;
DOI:10.1016/j.tet.2009.02.065

Reference yield: 69.0%

: 1187567-03-8
2-[N-(tert-butyloxycarbonyl)-N-(3-chloroprop-2-en-1-yl)-amino]-4-benzyloxy-1,9-dibromoanthracene

: 1187567-04-9
5-(benzyloxy)-3-(tert-butyloxycarbonyl)-1-(chloromethyl)-1,2-dihydronaphtho[2,3-e]indole

Guidance literature:: With 2,2'-azobis(isobutyronitrile); tri-n-butyl-tin hydride; In toluene; at 105 ℃; for 3h; Inert atmosphere;
DOI:10.1016/j.tet.2009.02.065