C₂₉H₃₄O₁₀

Base Information

Chemical Name:C₂₉H₃₄O₁₀
CAS No.:1316670-11-7
Molecular Formula:C₂₉H₃₄O₁₀
Molecular Weight:542.583
Hs Code.:

C<sub>29</sub>H<sub>34</sub>O<sub>10</sub>

Synonyms:C₂₉H₃₄O₁₀

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Chemical Property of C₂₉H₃₄O₁₀

Chemical Property:

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Technology Process of C₂₉H₃₄O₁₀

There total 26 articles about C₂₉H₃₄O₁₀ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 81.0%

: 1315567-63-5
des-epoxy-yuanhuapin

: 1316670-11-7
C₂₉H₃₄O₁₀

Guidance literature:: With tert.-butylhydroperoxide; (1S,2S)-N,N'-dihydroxy-N,N'-bis(3,3,3-triphenylpropionyl)-1,2-cyclohexadiamine; vanadium(V) oxytriisopropoxide; In dichloromethane; benzene; at 4 ℃;
DOI:10.1038/nchem.1074

Reference yield:

: 1315567-75-9
C₄₁H₄₄O₁₂

: 1316670-11-7
C₂₉H₃₄O₁₀

Guidance literature:: Multi-step reaction with 15 steps

1.1: sodium hydrogencarbonate; Dess-Martin periodane / dichloromethane / 20 °C

2.1: cerium(III) chloride / tetrahydrofuran / -78 °C

3.1: potassium carbonate / methanol; water / 50 °C

3.2: 0 °C

4.1: 2,6-dimethylpyridine; trifluoromethylsulfonic anhydride / dichloromethane / -78 °C

4.2: 65 °C

5.1: ammonium chloride; zinc / ethanol / 160 °C / Microwave irradiation

6.1: pyridinium p-toluenesulfonate / dichloromethane / 40 °C

7.1: N-Bromosuccinimide; sodium hydrogencarbonate; dibenzoyl peroxide / tetrachloromethane; benzene / 70 °C

7.2: 20 °C

8.1: lithium aluminium tetrahydride / tetrahydrofuran / 0 - 20 °C

9.1: dmap; triethylamine / dichloromethane / 20 °C

10.1: toluene-4-sulfonic acid / methanol; N,N-dimethyl-formamide / 200 °C / Microwave irradiation

11.1: dmap / dichloromethane / 20 °C

12.1: tris(dimethylamino)sulfonium trimethylsilyldifluoride / N,N-dimethyl-formamide / 20 °C

13.1: 1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione / dimethyl sulfoxide; toluene / 70 °C

14.1: potassium carbonate / methanol / 20 °C

14.2: 70 °C

15.1: tert.-butylhydroperoxide; (1S,2S)-N,N'-dihydroxy-N,N'-bis(3,3,3-triphenylpropionyl)-1,2-cyclohexadiamine; vanadium(V) oxytriisopropoxide / dichloromethane; benzene / 4 °C

With 2,6-dimethylpyridine; tert.-butylhydroperoxide; dmap; N-Bromosuccinimide; lithium aluminium tetrahydride; cerium(III) chloride; trifluoromethylsulfonic anhydride; (1S,2S)-N,N'-dihydroxy-N,N'-bis(3,3,3-triphenylpropionyl)-1,2-cyclohexadiamine; tris(dimethylamino)sulfonium trimethylsilyldifluoride; vanadium(V) oxytriisopropoxide; pyridinium p-toluenesulfonate; sodium hydrogencarbonate; potassium carbonate; ammonium chloride; Dess-Martin periodane; toluene-4-sulfonic acid; triethylamine; zinc; 1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione; dibenzoyl peroxide; In tetrahydrofuran; methanol; tetrachloromethane; ethanol; dichloromethane; water; dimethyl sulfoxide; N,N-dimethyl-formamide; toluene; benzene;
DOI:10.1038/nchem.1074

Reference yield:

: 1315567-64-6
C₄₄H₄₈O₁₂

: 1316670-11-7
C₂₉H₃₄O₁₀

Guidance literature:: Multi-step reaction with 13 steps

1.1: potassium carbonate / methanol; water / 50 °C

1.2: 0 °C

2.1: 2,6-dimethylpyridine; trifluoromethylsulfonic anhydride / dichloromethane / -78 °C

2.2: 65 °C

3.1: ammonium chloride; zinc / ethanol / 160 °C / Microwave irradiation

4.1: pyridinium p-toluenesulfonate / dichloromethane / 40 °C

5.1: N-Bromosuccinimide; sodium hydrogencarbonate; dibenzoyl peroxide / tetrachloromethane; benzene / 70 °C

5.2: 20 °C

6.1: lithium aluminium tetrahydride / tetrahydrofuran / 0 - 20 °C

7.1: dmap; triethylamine / dichloromethane / 20 °C

8.1: toluene-4-sulfonic acid / methanol; N,N-dimethyl-formamide / 200 °C / Microwave irradiation

9.1: dmap / dichloromethane / 20 °C

10.1: tris(dimethylamino)sulfonium trimethylsilyldifluoride / N,N-dimethyl-formamide / 20 °C

11.1: 1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione / dimethyl sulfoxide; toluene / 70 °C

12.1: potassium carbonate / methanol / 20 °C

12.2: 70 °C

13.1: tert.-butylhydroperoxide; (1S,2S)-N,N'-dihydroxy-N,N'-bis(3,3,3-triphenylpropionyl)-1,2-cyclohexadiamine; vanadium(V) oxytriisopropoxide / dichloromethane; benzene / 4 °C

With 2,6-dimethylpyridine; tert.-butylhydroperoxide; dmap; N-Bromosuccinimide; lithium aluminium tetrahydride; trifluoromethylsulfonic anhydride; (1S,2S)-N,N'-dihydroxy-N,N'-bis(3,3,3-triphenylpropionyl)-1,2-cyclohexadiamine; tris(dimethylamino)sulfonium trimethylsilyldifluoride; vanadium(V) oxytriisopropoxide; pyridinium p-toluenesulfonate; sodium hydrogencarbonate; potassium carbonate; ammonium chloride; toluene-4-sulfonic acid; triethylamine; zinc; 1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione; dibenzoyl peroxide; In tetrahydrofuran; methanol; tetrachloromethane; ethanol; dichloromethane; water; dimethyl sulfoxide; N,N-dimethyl-formamide; toluene; benzene;
DOI:10.1038/nchem.1074