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C51H56O17

Base Information
  • Chemical Name:C51H56O17
  • CAS No.:130719-12-9
  • Molecular Formula:C51H56O17
  • Molecular Weight:940.995
  • Hs Code.:
C<sub>51</sub>H<sub>56</sub>O<sub>17</sub>

Synonyms:C51H56O17

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Chemical Property of C51H56O17
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Technology Process of C51H56O17

There total 8 articles about C51H56O17 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:
Guidance literature:
With hydrazinium monoacetate; In methanol; water; at 50 ℃; for 4h;
Guidance literature:
Multi-step reaction with 8 steps
1: pyridine / 1 h / 0 °C
2: HOAc, H2O / 4 h / 60 °C
3: 89 percent / pyridine / dioxane / 1 h / 0 °C
4: 95 percent / NaHCO3 / dimethylformamide / 2 h / 20 °C
5: 84 percent / N-iodosuccinimide / trifluoromethanesulfonic acid / 1,2-dichloro-ethane / 0.08 h / 20 °C
6: 87 percent / hydrazine acetate / methanol; H2O / 4 h / 50 °C
7: 95 percent / N-iodosuccinimide / trifluoromethanesulfonic acid / 1,2-dichloro-ethane / 0.08 h / 0 °C
8: 80 percent / hydrazine acetate / methanol; H2O / 4 h / 50 °C
With pyridine; N-iodo-succinimide; water; hydrazinium monoacetate; sodium hydrogencarbonate; acetic acid; trifluorormethanesulfonic acid; In 1,4-dioxane; methanol; water; 1,2-dichloro-ethane; N,N-dimethyl-formamide;
Guidance literature:
Multi-step reaction with 9 steps
1: 63 percent / molecular sieves 4 Angstroem, HgCl2, HgO / acetonitrile / 0.08 h / 20 °C
2: pyridine / 1 h / 0 °C
3: HOAc, H2O / 4 h / 60 °C
4: 89 percent / pyridine / dioxane / 1 h / 0 °C
5: 95 percent / NaHCO3 / dimethylformamide / 2 h / 20 °C
6: 84 percent / N-iodosuccinimide / trifluoromethanesulfonic acid / 1,2-dichloro-ethane / 0.08 h / 20 °C
7: 87 percent / hydrazine acetate / methanol; H2O / 4 h / 50 °C
8: 95 percent / N-iodosuccinimide / trifluoromethanesulfonic acid / 1,2-dichloro-ethane / 0.08 h / 0 °C
9: 80 percent / hydrazine acetate / methanol; H2O / 4 h / 50 °C
With pyridine; N-iodo-succinimide; 4 A molecular sieve; water; hydrazinium monoacetate; sodium hydrogencarbonate; acetic acid; mercury dichloride; mercury(II) oxide; trifluorormethanesulfonic acid; In 1,4-dioxane; methanol; water; 1,2-dichloro-ethane; N,N-dimethyl-formamide; acetonitrile;
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