6-monomethoxytrityloxy-6'-hydroxy-bis-(hexanoylhydrazinocarbonyl-2-oxyethyl)sulfone

Base Information

Chemical Name:6-monomethoxytrityloxy-6'-hydroxy-bis-(hexanoylhydrazinocarbonyl-2-oxyethyl)sulfone
CAS No.:873694-56-5
Molecular Formula:C₃₈H₅₀N₄O₁₁S
Molecular Weight:770.901
Hs Code.:

Synonyms:6-monomethoxytrityloxy-6'-hydroxy-bis-(hexanoylhydrazinocarbonyl-2-oxyethyl)sulfone

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Chemical Property of 6-monomethoxytrityloxy-6'-hydroxy-bis-(hexanoylhydrazinocarbonyl-2-oxyethyl)sulfone

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Technology Process of 6-monomethoxytrityloxy-6'-hydroxy-bis-(hexanoylhydrazinocarbonyl-2-oxyethyl)sulfone

There total 4 articles about 6-monomethoxytrityloxy-6'-hydroxy-bis-(hexanoylhydrazinocarbonyl-2-oxyethyl)sulfone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 49.7%

: 873694-55-4
bis-[(6-hydroxyhexanoyl)hydrazinocarbonyl-2-oxyethyl]sulfone

: 14470-28-1
mono-4-methoxytrityl chloride

: 873694-56-5
6-monomethoxytrityloxy-6'-hydroxy-bis-(hexanoylhydrazinocarbonyl-2-oxyethyl)sulfone

Guidance literature:: With pyridine; In dichloromethane; at 20 ℃; for 3h;
DOI:10.1081/NCN-200055723

Reference yield:

: 502-44-3,24980-41-4,80137-66-2
hexahydro-2H-oxepin-2-one

: 873694-56-5
6-monomethoxytrityloxy-6'-hydroxy-bis-(hexanoylhydrazinocarbonyl-2-oxyethyl)sulfone

Guidance literature:: Multi-step reaction with 3 steps

1: 97 percent / aq. hydrazine / ethanol / 12 h / Heating

2: 65.2 percent / pyridine; DMAP / dimethylformamide / 20 h / 20 °C

3: 49.7 percent / pyridine / CH₂Cl₂ / 3 h / 20 °C

With pyridine; dmap; hydrazine hydrate; In ethanol; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1081/NCN-200055723

Reference yield:

: 1694-83-3
6-hydroxyhexanoic hydrazide

: 873694-56-5
6-monomethoxytrityloxy-6'-hydroxy-bis-(hexanoylhydrazinocarbonyl-2-oxyethyl)sulfone

Guidance literature:: Multi-step reaction with 2 steps

1: 65.2 percent / pyridine; DMAP / dimethylformamide / 20 h / 20 °C

2: 49.7 percent / pyridine / CH₂Cl₂ / 3 h / 20 °C

With pyridine; dmap; In dichloromethane; N,N-dimethyl-formamide;
DOI:10.1081/NCN-200055723