N⁶-benzyloxycarbonyl-N²-[N⁶-benzyloxycarbonyl-N²-(N²,N⁶-bis-benzyloxycarbonyl-L-lysyl)-L-lysyl]-L-lysine

Base Information

• Chemical Name: N⁶-benzyloxycarbonyl-N²-[N⁶-benzyloxycarbonyl-N²-(N²,N⁶-bis-benzyloxycarbonyl-L-lysyl)-L-lysyl]-L-lysine
• CAS No.: 120207-81-0
• Molecular Formula: C₅₀H₆₂N₆O₁₂
• Molecular Weight: 939.075

Synonyms:N⁶-benzyloxycarbonyl-N²-[N⁶-benzyloxycarbonyl-N²-(N²,N⁶-bis-benzyloxycarbonyl-L-lysyl)-L-lysyl]-L-lysine

Chemical Property of N⁶-benzyloxycarbonyl-N²-[N⁶-benzyloxycarbonyl-N²-(N²,N⁶-bis-benzyloxycarbonyl-L-lysyl)-L-lysyl]-L-lysine

Chemical Property:

Purity/Quality:

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Technology Process of N⁶-benzyloxycarbonyl-N²-[N⁶-benzyloxycarbonyl-N²-(N²,N⁶-bis-benzyloxycarbonyl-L-lysyl)-L-lysyl]-L-lysine

There total 9 articles about N⁶-benzyloxycarbonyl-N²-[N⁶-benzyloxycarbonyl-N²-(N²,N⁶-bis-benzyloxycarbonyl-L-lysyl)-L-lysyl]-L-lysine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

N6-benzyloxycarbonyl-N2-[N6-benzyloxycarbonyl-N2-(N2,N6-bis-benzyloxycarbonyl-L-lysyl)-L-lysyl]-L-lysine methyl ester (122701-29-5) → N6-benzyloxycarbonyl-N2-[N6-benzyloxycarbonyl-N2-(N2,N6-bis-benzyloxycarbonyl-L-lysyl)-L-lysyl]-L-lysine (120207-81-0)

Guidance literature:

With sodium hydroxide; acetone;

DOI:10.1039/jr9530000475

Reference yield:

N,N'-di-[(phenylmethoxy)carbonyl]-L-lysine (405-39-0) → N6-benzyloxycarbonyl-N2-[N6-benzyloxycarbonyl-N2-(N2,N6-bis-benzyloxycarbonyl-L-lysyl)-L-lysyl]-L-lysine (120207-81-0)

Guidance literature:

Multi-step reaction with 4 steps

2: NaOH; aqueous acetone

3: 1-ethyl-piperidine; THF / anschliessend Behandeln mit N⁶-Benzyloxycarbonyl-L-lysin-methylester, Aethylacetat und wss. KHCO₃

4: NaOH; aqueous acetone

With tetrahydrofuran; 1-ethyl-piperidine; sodium hydroxide; acetone;

DOI:10.1039/jr9530000475

Reference yield:

N6-[(benzyloxy)carbonyl]-N2-{N 2,N6-bis[(benzyloxy)carbonyl]-L-lysyl}-L-lysine (614-02-8) → N6-benzyloxycarbonyl-N2-[N6-benzyloxycarbonyl-N2-(N2,N6-bis-benzyloxycarbonyl-L-lysyl)-L-lysyl]-L-lysine (120207-81-0)

Guidance literature:

Multi-step reaction with 2 steps

1: 1-ethyl-piperidine; THF / anschliessend Behandeln mit N⁶-Benzyloxycarbonyl-L-lysin-methylester, Aethylacetat und wss. KHCO₃

2: NaOH; aqueous acetone

With tetrahydrofuran; 1-ethyl-piperidine; sodium hydroxide; acetone;

DOI:10.1039/jr9530000475

upstream raw materials:

N⁶-benzyloxycarbonyl-N²-[N⁶-benzyloxycarbonyl-N²-(N²,N⁶-bis-benzyloxycarbonyl-L-lysyl)-L-lysyl]-L-lysine methyl ester

N,N'-di-[(phenylmethoxy)carbonyl]-L-lysine

(S)-methyl 2-amino-6-(benzyloxycarbonylamino)hexanoate

N⁶-[(benzyloxy)carbonyl]-N²-{N ²,N⁶-bis[(benzyloxy)carbonyl]-L-lysyl}-L-lysine

Downstream raw materials:

C₆₅H₇₄Br₂N₈O₁₁

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