terrt-butyl 4-{[4-(5-bromo-2-pyridyl)phenyl]sulfonyl}perhydro-2H-pyran-4-carboxylate

Base Information

Chemical Name:terrt-butyl 4-{[4-(5-bromo-2-pyridyl)phenyl]sulfonyl}perhydro-2H-pyran-4-carboxylate
CAS No.:639492-78-7
Molecular Formula:C₂₁H₂₄BrNO₅S
Molecular Weight:482.395
Hs Code.:

Synonyms:terrt-butyl 4-{[4-(5-bromo-2-pyridyl)phenyl]sulfonyl}perhydro-2H-pyran-4-carboxylate

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Chemical Property of terrt-butyl 4-{[4-(5-bromo-2-pyridyl)phenyl]sulfonyl}perhydro-2H-pyran-4-carboxylate

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Technology Process of terrt-butyl 4-{[4-(5-bromo-2-pyridyl)phenyl]sulfonyl}perhydro-2H-pyran-4-carboxylate

There total 1 articles about terrt-butyl 4-{[4-(5-bromo-2-pyridyl)phenyl]sulfonyl}perhydro-2H-pyran-4-carboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 25.0%

: 624-28-2
2,5-dibromopyridine

: 639491-69-3
tert-butyl {[4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)phenyl]sulfonyl}perhydro-2H-pyran-4-carboxylate

: 639492-78-7
terrt-butyl 4-{[4-(5-bromo-2-pyridyl)phenyl]sulfonyl}perhydro-2H-pyran-4-carboxylate

Guidance literature:: With sodium carbonate; (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; In ethanol; toluene; at 80 ℃;

Reference yield: 96.0%

: 639492-78-7
terrt-butyl 4-{[4-(5-bromo-2-pyridyl)phenyl]sulfonyl}perhydro-2H-pyran-4-carboxylate

: 40723-80-6,71215-70-8
1,1,1,2,2-pentafluoro-4-iodobutane

: 639492-80-1
tert-butyl 4-({4-[5-(3,3,4,4,4-pentafluorobutyl)-2-pyridyl]phenyl}sulfonyl)perhydro-2H-pyran-4-carboxylate

Guidance literature:: 1,1,1,2,2-pentafluoro-4-iodobutane; With copper; zinc; In DMF (N,N-dimethyl-formamide); benzene; at 60 ℃; for 3h;

terrt-butyl 4-{[4-(5-bromo-2-pyridyl)phenyl]sulfonyl}perhydro-2H-pyran-4-carboxylate; (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; In DMF (N,N-dimethyl-formamide); benzene; at 60 - 75 ℃;

Reference yield: 57.0%

: 639492-78-7
terrt-butyl 4-{[4-(5-bromo-2-pyridyl)phenyl]sulfonyl}perhydro-2H-pyran-4-carboxylate

: 461-17-6
1,1,1-trifluoro-4-iodo-butane

: 1373151-95-1
tert-butyl 4-({4-[5-(4,4,4-trifluorobutyl)pyridin-2-yl]phenyl}sulfonyl)tetrahydro-2H-pyran-4-carboxylate

Guidance literature:: 1,1,1-trifluoro-4-iodo-butane; With copper; zinc; In DMF (N,N-dimethyl-formamide); benzene; at 60 ℃; for 3h;

terrt-butyl 4-{[4-(5-bromo-2-pyridyl)phenyl]sulfonyl}perhydro-2H-pyran-4-carboxylate; (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; In DMF (N,N-dimethyl-formamide); benzene; at 75 ℃;