4-[(2-(N-(2-(benzyloxyimino)ethyl)-N-(2-propenoyl)amino)ethoxy)carbonyl]butanoic acid

Base Information

Chemical Name:4-[(2-(N-(2-(benzyloxyimino)ethyl)-N-(2-propenoyl)amino)ethoxy)carbonyl]butanoic acid
CAS No.:352463-56-0
Molecular Formula:C₁₉H₂₄N₂O₆
Molecular Weight:376.409
Hs Code.:

Synonyms:4-[(2-(N-(2-(benzyloxyimino)ethyl)-N-(2-propenoyl)amino)ethoxy)carbonyl]butanoic acid

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Chemical Property of 4-[(2-(N-(2-(benzyloxyimino)ethyl)-N-(2-propenoyl)amino)ethoxy)carbonyl]butanoic acid

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Technology Process of 4-[(2-(N-(2-(benzyloxyimino)ethyl)-N-(2-propenoyl)amino)ethoxy)carbonyl]butanoic acid

There total 4 articles about 4-[(2-(N-(2-(benzyloxyimino)ethyl)-N-(2-propenoyl)amino)ethoxy)carbonyl]butanoic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

: 108-55-4
glutaric anhydride,

: 294675-53-9
N-(2-hydroxyethyl)-N-[2-[(phenylmethoxy)imino]ethyl]-2-propenamide

: 352463-56-0
4-[(2-(N-(2-(benzyloxyimino)ethyl)-N-(2-propenoyl)amino)ethoxy)carbonyl]butanoic acid

Guidance literature:: With pyridine; at 80 ℃;
DOI:10.1039/b101074n

Reference yield: 93.0%

: 108-55-4
glutaric anhydride,

: 294675-53-9
N-(2-hydroxyethyl)-N-[2-[(phenylmethoxy)imino]ethyl]-2-propenamide

: 352463-56-0
4-[(2-(N-(2-(benzyloxyimino)ethyl)-N-(2-propenoyl)amino)ethoxy)carbonyl]butanoic acid

: pentanedioic acid mono-{2-[acryloyl-(2-hydroxyimino-ethyl)-amino]-ethyl} ester

Guidance literature:: With pyridine; at 100 ℃; for 4h;
DOI:10.1248/cpb.52.842

Reference yield:

: 101389-21-3
α-chloroacetaldoxime benzyl ether

: 352463-56-0
4-[(2-(N-(2-(benzyloxyimino)ethyl)-N-(2-propenoyl)amino)ethoxy)carbonyl]butanoic acid

Guidance literature:: Multi-step reaction with 3 steps

1: 88 percent / 20 °C

2: 87 percent / aq. Na₂CO₃ / acetone / 0 °C

3: 93 percent / pyridine / 80 °C

With pyridine; sodium carbonate; In acetone;
DOI:10.1039/b101074n