di-tert-butyl 1-(1-(4-bromophenyl)-2-oxocyclohexyl)hydrazine-1,2-dicarboxylate

Base Information

Chemical Name:di-tert-butyl 1-(1-(4-bromophenyl)-2-oxocyclohexyl)hydrazine-1,2-dicarboxylate
CAS No.:1070898-76-8
Molecular Formula:C₂₂H₃₁BrN₂O₅
Molecular Weight:483.403
Hs Code.:

Synonyms:di-tert-butyl 1-(1-(4-bromophenyl)-2-oxocyclohexyl)hydrazine-1,2-dicarboxylate

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Chemical Property of di-tert-butyl 1-(1-(4-bromophenyl)-2-oxocyclohexyl)hydrazine-1,2-dicarboxylate

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Technology Process of di-tert-butyl 1-(1-(4-bromophenyl)-2-oxocyclohexyl)hydrazine-1,2-dicarboxylate

There total 2 articles about di-tert-butyl 1-(1-(4-bromophenyl)-2-oxocyclohexyl)hydrazine-1,2-dicarboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

: 1070898-70-2
C₁₃H₁₅BrO₂

: 870-50-8
di-tert-butyl (E)-azodicarboxylate

: 1070898-76-8
di-tert-butyl 1-(1-(4-bromophenyl)-2-oxocyclohexyl)hydrazine-1,2-dicarboxylate

Guidance literature:: With N,N,N,N,N,N-hexamethylphosphoric triamide; samarium diiodide; In tetrahydrofuran; at 20 ℃; for 1h;
DOI:10.1016/j.tetlet.2008.07.123

Reference yield:

: 870-50-8
di-tert-butyl-diazodicarboxylate

: 91720-92-2
2-(4-bromophenyl)cyclohexan-1-one

: 1070898-76-8
di-tert-butyl 1-(1-(4-bromophenyl)-2-oxocyclohexyl)hydrazine-1,2-dicarboxylate

Guidance literature:: With (R)-3,3'-bis(2,4,6-triisopropylphenyl)-1,1'-binaphthyl-2,2'-diylhydrogenphosphate; In neat (no solvent); at 45 ℃; for 60h; enantioselective reaction;
DOI:10.1021/jacs.5b00229