N-{4-[1-(4-amino-3,5-dimethyl-phenyl)-cyclohexyl]-2,6-dimethyl-phenyl}-N'-(2,6-diisopropyl-phenyl)-isophthalamide

Base Information

Chemical Name:N-{4-[1-(4-amino-3,5-dimethyl-phenyl)-cyclohexyl]-2,6-dimethyl-phenyl}-N'-(2,6-diisopropyl-phenyl)-isophthalamide
CAS No.:299173-87-8
Molecular Formula:C₄₂H₅₁N₃O₂
Molecular Weight:629.886
Hs Code.:

<i>N</i>-{4-[1-(4-amino-3,5-dimethyl-phenyl)-cyclohexyl]-2,6-dimethyl-phenyl}-<i>N</i>'-(2,6-diisopropyl-phenyl)-isophthalamide

Synonyms:N-{4-[1-(4-amino-3,5-dimethyl-phenyl)-cyclohexyl]-2,6-dimethyl-phenyl}-N'-(2,6-diisopropyl-phenyl)-isophthalamide

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Chemical Property of N-{4-[1-(4-amino-3,5-dimethyl-phenyl)-cyclohexyl]-2,6-dimethyl-phenyl}-N'-(2,6-diisopropyl-phenyl)-isophthalamide

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Technology Process of N-{4-[1-(4-amino-3,5-dimethyl-phenyl)-cyclohexyl]-2,6-dimethyl-phenyl}-N'-(2,6-diisopropyl-phenyl)-isophthalamide

There total 3 articles about N-{4-[1-(4-amino-3,5-dimethyl-phenyl)-cyclohexyl]-2,6-dimethyl-phenyl}-N'-(2,6-diisopropyl-phenyl)-isophthalamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 22657-66-5
1,1-bis(4-amino-3,5-dimethylphenyl)cyclohexane

: 299173-85-6
3-{N-[(2,6-diisopropyl)phenyl]formamido}benzoyl chloride

: 299173-87-8
N-{4-[1-(4-amino-3,5-dimethyl-phenyl)-cyclohexyl]-2,6-dimethyl-phenyl}-N'-(2,6-diisopropyl-phenyl)-isophthalamide

Guidance literature:: With triethylamine; In dichloromethane; for 5h;
DOI:10.1021/ja0012671

Reference yield:

: 24544-04-5
2,6-diisopropylbenzenamine

: 299173-87-8
N-{4-[1-(4-amino-3,5-dimethyl-phenyl)-cyclohexyl]-2,6-dimethyl-phenyl}-N'-(2,6-diisopropyl-phenyl)-isophthalamide

Guidance literature:: Multi-step reaction with 2 steps

1: 86 percent / Et₃N / CH₂Cl₂ / 20 h / 20 °C

2: 85 percent / Et₃N / CH₂Cl₂ / 5 h

With triethylamine; In dichloromethane;
DOI:10.1021/ja0012671

Reference yield:

: 99-63-8
benzene-1,3-dicarbonyl dichloride

: 299173-87-8
N-{4-[1-(4-amino-3,5-dimethyl-phenyl)-cyclohexyl]-2,6-dimethyl-phenyl}-N'-(2,6-diisopropyl-phenyl)-isophthalamide

Guidance literature:: Multi-step reaction with 2 steps

1: 86 percent / Et₃N / CH₂Cl₂ / 20 h / 20 °C

2: 85 percent / Et₃N / CH₂Cl₂ / 5 h

With triethylamine; In dichloromethane;
DOI:10.1021/ja0012671