2-(trimethylsilyl)-6-silyl>benzenethiol

Base Information

Chemical Name:2-(trimethylsilyl)-6-silyl>benzenethiol
CAS No.:117526-67-7
Molecular Formula:C₁₅H₃₀SSi₃
Molecular Weight:326.726
Hs Code.:

2-(trimethylsilyl)-6-<dimethyl<(trimethylsilyl)methyl>silyl>benzenethiol

Synonyms:2-(trimethylsilyl)-6-silyl>benzenethiol

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Chemical Property of 2-(trimethylsilyl)-6-silyl>benzenethiol

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Technology Process of 2-(trimethylsilyl)-6-silyl>benzenethiol

There total 3 articles about 2-(trimethylsilyl)-6-silyl>benzenethiol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 108-98-5
thiophenol

: 117526-67-7
2-(trimethylsilyl)-6-silyl>benzenethiol

Guidance literature:: Multi-step reaction with 4 steps

1: 92 percent / pyridinium p-toluenesulfonate / CH₂Cl₂ / 4 h / 25 °C

2: 1.) t-BuLi / 1.) THF, HMPA, -95 deg C, 2 h, 2.) 25 deg C

3: 1.) K₂CO₃, aq. AgNO₃, 2.) H₂S / 1.) MeOH, 3 h, 2.) CH₂Cl₂, 1.5 h

With hydrogen sulfide; tert.-butyl lithium; pyridinium p-toluenesulfonate; potassium carbonate; silver nitrate; In dichloromethane;
DOI:10.1021/ja00184a039

Reference yield:

: 20965-36-0
2-(phenylthio)tetrahydro-2H-pyran

: 117526-67-7
2-(trimethylsilyl)-6-silyl>benzenethiol

Guidance literature:: Multi-step reaction with 3 steps

1: 1.) t-BuLi / 1.) THF, HMPA, -95 deg C, 2 h, 2.) 25 deg C

2: 1.) K₂CO₃, aq. AgNO₃, 2.) H₂S / 1.) MeOH, 3 h, 2.) CH₂Cl₂, 1.5 h

With hydrogen sulfide; tert.-butyl lithium; potassium carbonate; silver nitrate;
DOI:10.1021/ja00184a039

Reference yield:

: 117526-61-1
2-(trimethylsilyl)phenyl-2-tetrahydropyranyl sulfide

: 117526-67-7
2-(trimethylsilyl)-6-silyl>benzenethiol

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) K₂CO₃, aq. AgNO₃, 2.) H₂S / 1.) MeOH, 3 h, 2.) CH₂Cl₂, 1.5 h

With hydrogen sulfide; potassium carbonate; silver nitrate;
DOI:10.1021/ja00184a039