Carbamic acid, [(1S,2R)-2-hydroxy-1-methyl-2-phenylethyl]-, methyl ester

Base Information

Chemical Name:Carbamic acid, [(1S,2R)-2-hydroxy-1-methyl-2-phenylethyl]-, methyl ester
CAS No.:113323-00-5
Molecular Formula:C₁₁H₁₅NO₃
Molecular Weight:209.245
Hs Code.:
DSSTox Substance ID:DTXSID101149236

Synonyms:DTXSID101149236;Carbamic acid, [(1S,2R)-2-hydroxy-1-methyl-2-phenylethyl]-, methyl ester;113323-00-5

Suppliers and Price of Carbamic acid, [(1S,2R)-2-hydroxy-1-methyl-2-phenylethyl]-, methyl ester

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Carbamic acid, [(1S,2R)-2-hydroxy-1-methyl-2-phenylethyl]-, methyl ester

Chemical Property:

XLogP3:1.2
Hydrogen Bond Donor Count:2
Hydrogen Bond Acceptor Count:3
Rotatable Bond Count:4
Exact Mass:209.10519334
Heavy Atom Count:15
Complexity:202

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:CC(C(C1=CC=CC=C1)O)NC(=O)OC
Isomeric SMILES:C[C@@H]([C@@H](C1=CC=CC=C1)O)NC(=O)OC

Technology Process of Carbamic acid, [(1S,2R)-2-hydroxy-1-methyl-2-phenylethyl]-, methyl ester

There total 3 articles about Carbamic acid, [(1S,2R)-2-hydroxy-1-methyl-2-phenylethyl]-, methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

: 77447-97-3
(S)-2-<(Methoxycarbonyl)amino>-1-phenylpropanone

: 113323-00-5
(1R,2S)-2-<(methoxycarbonyl)amino>-1-phenyl-1-propanol

Guidance literature:: With Dimethylphenylsilane; trifluoroacetic acid; at 0 ℃; for 4h;
DOI:10.1021/jo00258a004

Reference yield:

: phenylmagnesium bromide

: 113323-00-5
(1R,2S)-2-<(methoxycarbonyl)amino>-1-phenyl-1-propanol

Guidance literature:: Multi-step reaction with 2 steps

1: 99 percent / tetrahydrofuran / 3 h

2: 87 percent / PhMe₂SiH, CF₃COOH / 4 h / 0 °C

With Dimethylphenylsilane; trifluoroacetic acid; In tetrahydrofuran;
DOI:10.1021/jo00258a004

Reference yield:

: 91110-99-5
(S)-N,N-dimethyl-2-<(methoxycarbonyl)amino>propanamide

: 113323-00-5
(1R,2S)-2-<(methoxycarbonyl)amino>-1-phenyl-1-propanol

Guidance literature:: Multi-step reaction with 2 steps

1: 99 percent / tetrahydrofuran / 3 h

2: 87 percent / PhMe₂SiH, CF₃COOH / 4 h / 0 °C

With Dimethylphenylsilane; trifluoroacetic acid; In tetrahydrofuran;
DOI:10.1021/jo00258a004