1-((tert-butoxy)carbonyl)-4-(phenylthio)-1,2,5,6-tetrahydro-2-pyridinone

Base Information

Chemical Name:1-((tert-butoxy)carbonyl)-4-(phenylthio)-1,2,5,6-tetrahydro-2-pyridinone
CAS No.:1420778-98-8
Molecular Formula:C₁₆H₁₉NO₃S
Molecular Weight:305.398
Hs Code.:

Synonyms:1-((tert-butoxy)carbonyl)-4-(phenylthio)-1,2,5,6-tetrahydro-2-pyridinone

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Chemical Property of 1-((tert-butoxy)carbonyl)-4-(phenylthio)-1,2,5,6-tetrahydro-2-pyridinone

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Technology Process of 1-((tert-butoxy)carbonyl)-4-(phenylthio)-1,2,5,6-tetrahydro-2-pyridinone

There total 1 articles about 1-((tert-butoxy)carbonyl)-4-(phenylthio)-1,2,5,6-tetrahydro-2-pyridinone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

: 24424-99-5
di-tert-butyl dicarbonate

: 411240-92-1
4-phenylsulfanyl-5,6-dihydro-1H-pyridin-2-one

: 1420778-98-8
1-((tert-butoxy)carbonyl)-4-(phenylthio)-1,2,5,6-tetrahydro-2-pyridinone

Guidance literature:: With dmap; triethylamine; In dichloromethane; at 20 ℃; for 3h; Inert atmosphere;
DOI:10.1016/j.tet.2012.12.017

Reference yield: 91.0%

: 1420778-98-8
1-((tert-butoxy)carbonyl)-4-(phenylthio)-1,2,5,6-tetrahydro-2-pyridinone

: 1420779-02-7
1-((tert-butoxy)carbonyl)-4-(phenylsulfonyl)-1,2,5,6-tetrahydro-2-pyridinone

Guidance literature:: With 3-chloro-benzenecarboperoxoic acid; In dichloromethane; water; at 20 ℃; for 2h;
DOI:10.1016/j.tet.2012.12.017

Reference yield:

: 1420778-98-8
1-((tert-butoxy)carbonyl)-4-(phenylthio)-1,2,5,6-tetrahydro-2-pyridinone

: 1420779-10-7
2-allyl-4-(phenylsulfonyl)-1,2,5,6-tetrahydropyridine

Guidance literature:: Multi-step reaction with 3 steps

1.1: 3-chloro-benzenecarboperoxoic acid / dichloromethane; water / 2 h / 20 °C

2.1: dichloromethane; tetrahydrofuran / -78 °C

3.1: boron trifluoride diethyl etherate / dichloromethane / 0.5 h / -78 °C

3.2: -78 - 20 °C

With boron trifluoride diethyl etherate; 3-chloro-benzenecarboperoxoic acid; In tetrahydrofuran; dichloromethane; water;
DOI:10.1016/j.tet.2012.12.017