dichlorido{N-[2-(diphenylphosphanyl)benzylidene]-2-methylaniline}-palladium(II)

Base Information

Chemical Name:dichlorido{N-[2-(diphenylphosphanyl)benzylidene]-2-methylaniline}-palladium(II)
CAS No.:1433901-83-7
Molecular Formula:C₂₆H₂₂Cl₂NPPd
Molecular Weight:556.767
Hs Code.:

Synonyms:dichlorido{N-[2-(diphenylphosphanyl)benzylidene]-2-methylaniline}-palladium(II)

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Chemical Property of dichlorido{N-[2-(diphenylphosphanyl)benzylidene]-2-methylaniline}-palladium(II)

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Technology Process of dichlorido{N-[2-(diphenylphosphanyl)benzylidene]-2-methylaniline}-palladium(II)

There total 4 articles about dichlorido{N-[2-(diphenylphosphanyl)benzylidene]-2-methylaniline}-palladium(II) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 81.0%

: 12107-56-1
dichloro(1,5-cyclooctadiene)palladium(II)

: 1433889-39-4
(2-diphenylphosphinobenzylidene)-2-methylphenylenamine

: 1433901-83-7
dichlorido{N-[2-(diphenylphosphanyl)benzylidene]-2-methylaniline}-palladium(II)

Guidance literature:: In dichloromethane; at 20 ℃; for 4h; Schlenk technique; Inert atmosphere;
DOI:10.1002/aoc.3158

Reference yield:

: 50777-76-9
(2-formylphenyl)(diphenyl)phosphine

: 1433901-83-7
dichlorido{N-[2-(diphenylphosphanyl)benzylidene]-2-methylaniline}-palladium(II)

Guidance literature:: Multi-step reaction with 2 steps

1: magnesium sulfate / dichloromethane / 20 °C / Inert atmosphere; Schlenk technique

2: dichloromethane / 6 h / 20 °C / Inert atmosphere; Schlenk technique

With magnesium sulfate; In dichloromethane; 1: |Schiff Reaction;
DOI:10.1016/j.jinorgbio.2013.09.010

Reference yield:

: 50777-76-9
(2-formylphenyl)(diphenyl)phosphine

: 95-53-4
o-toluidine

: 1433901-83-7
dichlorido{N-[2-(diphenylphosphanyl)benzylidene]-2-methylaniline}-palladium(II)

Guidance literature:: Multi-step reaction with 2 steps

1: formic acid / dichloromethane / 2 h / Schlenk technique; Inert atmosphere; Reflux

2: dichloromethane / 4 h / 20 °C / Schlenk technique; Inert atmosphere

With formic acid; In dichloromethane;
DOI:10.1002/aoc.3158