benzyl endo-7-(2-methanesulfonyloxyethyl)-6-oxo-2-azabicyclo<2.2.2>octane-2-carboxylate

Base Information

Chemical Name:benzyl endo-7-(2-methanesulfonyloxyethyl)-6-oxo-2-azabicyclo<2.2.2>octane-2-carboxylate
CAS No.:105594-72-7
Molecular Formula:C₁₈H₂₃NO₆S
Molecular Weight:381.45
Hs Code.:

Synonyms:benzyl endo-7-(2-methanesulfonyloxyethyl)-6-oxo-2-azabicyclo<2.2.2>octane-2-carboxylate

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Chemical Property of benzyl endo-7-(2-methanesulfonyloxyethyl)-6-oxo-2-azabicyclo<2.2.2>octane-2-carboxylate

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Technology Process of benzyl endo-7-(2-methanesulfonyloxyethyl)-6-oxo-2-azabicyclo<2.2.2>octane-2-carboxylate

There total 3 articles about benzyl endo-7-(2-methanesulfonyloxyethyl)-6-oxo-2-azabicyclo<2.2.2>octane-2-carboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: 81127-37-9,81176-97-8
benzyl endo-7-(2-methanesulfonyloxyethyl)-6,6-dimethoxy-2-azabicyclo<2.2.2>octane-2-carboxylate

: 105594-72-7
benzyl endo-7-(2-methanesulfonyloxyethyl)-6-oxo-2-azabicyclo<2.2.2>octane-2-carboxylate

Guidance literature:: With hydrogenchloride; In acetone; for 0.5h; Heating;

Reference yield:

: 81127-36-8,81176-96-7
benzyl endo-7-(2-hydroxyethyl)-6,6-dimethoxy-2-azabicyclo<2.2.2>octane-2-carboxylate

: 105594-72-7
benzyl endo-7-(2-methanesulfonyloxyethyl)-6-oxo-2-azabicyclo<2.2.2>octane-2-carboxylate

Guidance literature:: Multi-step reaction with 2 steps

1: 96 percent / Et₃N / benzene / 3 h / Ambient temperature

2: 92 percent / HCl / acetone / 0.5 h / Heating

With hydrogenchloride; triethylamine; In acetone; benzene;

Reference yield:

: 81127-35-7,81176-95-6
benzyl endo-7-ethoxycarbonylmethyl-6,6-dimethoxy-2-azabicyclo<2.2.2>octane-2-carboxylate

: 105594-72-7
benzyl endo-7-(2-methanesulfonyloxyethyl)-6-oxo-2-azabicyclo<2.2.2>octane-2-carboxylate

Guidance literature:: Multi-step reaction with 3 steps

1: 92 percent / LiAlH₄ / diethyl ether / 0.5 h / ice cooling

2: 96 percent / Et₃N / benzene / 3 h / Ambient temperature

3: 92 percent / HCl / acetone / 0.5 h / Heating

With hydrogenchloride; lithium aluminium tetrahydride; triethylamine; In diethyl ether; acetone; benzene;