6-(4-cinnamoylphenoxy)-hexyl α-D-galactopyranosyl-(1->3)-β-D-galactopyranosyl-(1->4)-β-D-glucopyranoside

Base Information

Chemical Name:6-(4-cinnamoylphenoxy)-hexyl α-D-galactopyranosyl-(1->3)-β-D-galactopyranosyl-(1->4)-β-D-glucopyranoside
CAS No.:909543-68-6
Molecular Formula:C₃₉H₅₄O₁₈
Molecular Weight:810.847
Hs Code.:

Synonyms:6-(4-cinnamoylphenoxy)-hexyl α-D-galactopyranosyl-(1->3)-β-D-galactopyranosyl-(1->4)-β-D-glucopyranoside

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Chemical Property of 6-(4-cinnamoylphenoxy)-hexyl α-D-galactopyranosyl-(1->3)-β-D-galactopyranosyl-(1->4)-β-D-glucopyranoside

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Technology Process of 6-(4-cinnamoylphenoxy)-hexyl α-D-galactopyranosyl-(1->3)-β-D-galactopyranosyl-(1->4)-β-D-glucopyranoside

There total 5 articles about 6-(4-cinnamoylphenoxy)-hexyl α-D-galactopyranosyl-(1->3)-β-D-galactopyranosyl-(1->4)-β-D-glucopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 77.0%

: 909543-81-3
6-chlorohexyl 4-O-[3-O-(α-D-galactopyranosyl)-β-D-galactopyranosyl]-1-β-D-glucopyranoside

: 2657-25-2
(E)-1-(4-hydroxyphenyl)-3-phenylprop-2-en-1-one

: 909543-68-6
6-(4-cinnamoylphenoxy)-hexyl α-D-galactopyranosyl-(1->3)-β-D-galactopyranosyl-(1->4)-β-D-glucopyranoside

Guidance literature:: With potassium carbonate; In N,N-dimethyl-formamide; at 95 - 100 ℃; for 24h;
DOI:10.1016/j.carres.2006.03.044

Reference yield:

: 909543-80-2
6-chloro-n-hexyl 2,3,4,6-tetra-O-acetyl-α-D-galactopyranosyl-(1->3)-2,4,6-tri-O-acetyl-β-D-galactopyranosyl-(1->4)-2,3,6-tri-O-acetyl-β-D-glucopyranoside

: 909543-68-6
6-(4-cinnamoylphenoxy)-hexyl α-D-galactopyranosyl-(1->3)-β-D-galactopyranosyl-(1->4)-β-D-glucopyranoside

Guidance literature:: Multi-step reaction with 2 steps

1: 100 percent / NaOMe / methanol / 20 °C

2: 77 percent / K₂CO₃ / dimethylformamide / 24 h / 95 - 100 °C

With sodium methylate; potassium carbonate; In methanol; N,N-dimethyl-formamide;
DOI:10.1016/j.carres.2006.03.044

Reference yield:

: 113421-54-8,113421-57-1
O-(2,3,4,6-tetra-O-acetyl-α-D-galactopyranosyl)-(1-3)-O-(2,4,6-tri-O-acetyl-β-D-galactopyranosyl)-(1-4)-2,3,6-tri-O-acetyl-α (and β)-D-glucopyranose

: 909543-68-6
6-(4-cinnamoylphenoxy)-hexyl α-D-galactopyranosyl-(1->3)-β-D-galactopyranosyl-(1->4)-β-D-glucopyranoside

Guidance literature:: Multi-step reaction with 4 steps

1: 82 percent / DBU / CH₂Cl₂ / 4 h / 20 °C

2: 44 percent / TMSOTf / acetonitrile / 2.5 h / -25 - 20 °C

3: 100 percent / NaOMe / methanol / 20 °C

4: 77 percent / K₂CO₃ / dimethylformamide / 24 h / 95 - 100 °C

With trimethylsilyl trifluoromethanesulfonate; sodium methylate; potassium carbonate; 1,8-diazabicyclo[5.4.0]undec-7-ene; In methanol; dichloromethane; N,N-dimethyl-formamide; acetonitrile;
DOI:10.1016/j.carres.2006.03.044