C₂₂H₂₀ClFN₂O₇

Base Information

Chemical Name:C₂₂H₂₀ClFN₂O₇
CAS No.:1251583-67-1
Molecular Formula:C₂₂H₂₀ClFN₂O₇
Molecular Weight:478.861
Hs Code.:

C<sub>22</sub>H<sub>20</sub>ClFN<sub>2</sub>O<sub>7</sub>

Synonyms:C₂₂H₂₀ClFN₂O₇

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Chemical Property of C₂₂H₂₀ClFN₂O₇

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Technology Process of C₂₂H₂₀ClFN₂O₇

There total 5 articles about C₂₂H₂₀ClFN₂O₇ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 63.0%

: 1251583-66-0
C₂₂H₂₂ClFN₂O₇

: 1251583-67-1
C₂₂H₂₀ClFN₂O₇

Guidance literature:: With Dess-Martin periodane; In dichloromethane; at 20 ℃; for 2h; Inert atmosphere;

Reference yield:

: 1251583-64-8
C₁₅H₁₈ClNO₄

: 1251583-67-1
C₂₂H₂₀ClFN₂O₇

Guidance literature:: Multi-step reaction with 2 steps

1.1: lithium diisopropyl amide / tetrahydrofuran; hexane; ethylbenzene / 0.33 h / -78 °C / Inert atmosphere

1.2: 0.17 h

2.1: Dess-Martin periodane / dichloromethane / 2 h / 20 °C / Inert atmosphere

With Dess-Martin periodane; lithium diisopropyl amide; In tetrahydrofuran; hexane; dichloromethane; ethylbenzene;

Reference yield:

: 1251584-47-0
C₁₈H₂₂ClNO₆

: 1251583-67-1
C₂₂H₂₀ClFN₂O₇

Guidance literature:: Multi-step reaction with 4 steps

1.1: water; potassium hydroxide / methanol / 2 h / Reflux

2.1: copper / quinoline / 2 h / 220 °C / Inert atmosphere; Microwave irradiation

3.1: lithium diisopropyl amide / tetrahydrofuran; hexane; ethylbenzene / 0.33 h / -78 °C / Inert atmosphere

3.2: 0.17 h

4.1: Dess-Martin periodane / dichloromethane / 2 h / 20 °C / Inert atmosphere

With water; copper; Dess-Martin periodane; potassium hydroxide; lithium diisopropyl amide; In tetrahydrofuran; quinoline; methanol; hexane; dichloromethane; ethylbenzene;