4-bromo-2,6-dinitroiodobenzene

Base Information

• Chemical Name: 4-bromo-2,6-dinitroiodobenzene
• CAS No.: 100191-18-2
• Molecular Formula: C₆H₂BrIN₂O₄
• Molecular Weight: 372.901
• Mol file: 100191-18-2.mol

Synonyms:4-bromo-2,6-dinitroiodobenzene

Chemical Property of 4-bromo-2,6-dinitroiodobenzene

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 4-bromo-2,6-dinitroiodobenzene

There total 3 articles about 4-bromo-2,6-dinitroiodobenzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 61.0%

4-bromo-2,6-dinitroaniline (62554-90-9) → 4-bromo-2,6-dinitroiodobenzene (100191-18-2)

Guidance literature:

4-bromo-2,6-dinitroaniline; With sulfuric acid; acetic acid; sodium nitrite; at 20 - 50 ℃; for 0.5h;

With potassium iodide; In water; at 70 ℃; for 0.25h;

DOI:10.1016/j.orgel.2018.12.027

Reference yield:

2,6-dinitroaniline (606-22-4) → 4-bromo-2,6-dinitroiodobenzene (100191-18-2)

Guidance literature:

Multi-step reaction with 2 steps

1.1: acetic acid; bromine / 2 h / 120 °C

2.1: acetic acid; sodium nitrite; sulfuric acid / 0.5 h / 20 - 50 °C

2.2: 0.25 h / 70 °C

With sulfuric acid; bromine; acetic acid; sodium nitrite;

DOI:10.1016/j.orgel.2018.12.027

Reference yield:

(4-bromo-2,6-dinitro-phenyl)-hydrazine (89581-43-1) → 4-bromo-2,6-dinitroiodobenzene (100191-18-2)

Guidance literature:

With ethanol; iodine;

upstream raw materials:

(4-bromo-2,6-dinitro-phenyl)-hydrazine

2,6-dinitroaniline

4-bromo-2,6-dinitroaniline