Technology Process of C64H70F6O4Si2
There total 5 articles about C64H70F6O4Si2 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
sodium hexamethyldisilazane;
In
tetrahydrofuran;
for 20h;
Inert atmosphere;
Reflux;
DOI:10.1246/cl.130190
- Guidance literature:
-
Multi-step reaction with 3 steps
1: trifluoroacetic anhydride / water / 1 h / 20 °C / Inert atmosphere
2: zinc / tetrahydrofuran / 2 h / 20 °C / Inert atmosphere
3: sodium hexamethyldisilazane / tetrahydrofuran / 20 h / Inert atmosphere; Reflux
With
sodium hexamethyldisilazane; trifluoroacetic anhydride; zinc;
In
tetrahydrofuran; water;
DOI:10.1246/cl.130190
- Guidance literature:
-
Multi-step reaction with 5 steps
1.1: benzene; methanol / 20 °C
2.1: magnesium / tetrahydrofuran / 1 h / Reflux; Inert atmosphere
2.2: 3.5 h / Inert atmosphere; Reflux
3.1: trifluoroacetic anhydride / water / 1 h / 20 °C / Inert atmosphere
4.1: zinc / tetrahydrofuran / 2 h / 20 °C / Inert atmosphere
5.1: sodium hexamethyldisilazane / tetrahydrofuran / 20 h / Inert atmosphere; Reflux
With
sodium hexamethyldisilazane; magnesium; trifluoroacetic anhydride; zinc;
In
tetrahydrofuran; methanol; water; benzene;
DOI:10.1246/cl.130190