2-[(1R,2R)-2,3-dihydroxy-1-(4-methylbenzoyloxy)propyl]pyridinium chloride

Base Information

• Chemical Name: 2-[(1R,2R)-2,3-dihydroxy-1-(4-methylbenzoyloxy)propyl]pyridinium chloride
• CAS No.: 1007352-81-9
• Molecular Formula: C₁₆H₁₇NO₄*ClH
• Molecular Weight: 323.776

Synonyms:2-[(1R,2R)-2,3-dihydroxy-1-(4-methylbenzoyloxy)propyl]pyridinium chloride

Chemical Property of 2-[(1R,2R)-2,3-dihydroxy-1-(4-methylbenzoyloxy)propyl]pyridinium chloride

Chemical Property:

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Technology Process of 2-[(1R,2R)-2,3-dihydroxy-1-(4-methylbenzoyloxy)propyl]pyridinium chloride

There total 1 articles about 2-[(1R,2R)-2,3-dihydroxy-1-(4-methylbenzoyloxy)propyl]pyridinium chloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

(1R)-1-[((4R)-2,2-dimethyl-1,3-dioxolan-4-yl)(pyridin-2-yl)]methyl 4-methylbenzoate (1007352-80-8) → 2-[(1R,2R)-2,3-dihydroxy-1-(4-methylbenzoyloxy)propyl]pyridinium chloride (1007352-81-9)

Guidance literature:

With hydrogenchloride; In 1,4-dioxane; at 20 ℃; for 2h;

DOI:10.1021/jo702141b

Reference yield: 99.0%

2-[(1R,2R)-2,3-dihydroxy-1-(4-methylbenzoyloxy)propyl]pyridinium chloride (1007352-81-9) → (1R,2R)-2-hydroxy-1-(4-methylbenzoyloxy)-2,3-dihydro-1H-indolizinium chloride (1007352-82-0)

Guidance literature:

With di-isopropyl azodicarboxylate; triphenylphosphine; In acetonitrile; at 20 ℃; for 2h;

DOI:10.1021/jo702141b

upstream raw materials:

(1R)-1-[((4R)-2,2-dimethyl-1,3-dioxolan-4-yl)(pyridin-2-yl)]methyl 4-methylbenzoate

Downstream raw materials:

(1R,2R)-2-hydroxy-1-(4-methylbenzoyloxy)-2,3-dihydro-1H-indolizinium chloride

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