N--(R)-serine methylester

Base Information

Chemical Name:N--(R)-serine methylester
CAS No.:155225-25-5
Molecular Formula:C₁₇H₂₄N₂O₆
Molecular Weight:352.387
Hs Code.:

N-<N'-(benzyloxycarbonyl)-(S)-valyl>-(R)-serine methylester

Synonyms:N--(R)-serine methylester

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N--(R)-serine methylester

Chemical Property:

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Technology Process of N--(R)-serine methylester

There total 6 articles about N--(R)-serine methylester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 53.0%

: 1149-26-4
(S)-N-(benzyloxycarbonyl)valine

: 5874-57-7
R-(-)-serine methyl ester hydrochloride

: 155225-25-5
N--(R)-serine methylester

Guidance literature:: With 4-methyl-morpholine; chloroformic acid ethyl ester; In ethyl acetate; -15 deg C, 1 h, then RT, 12 h;
DOI:10.1055/s-1994-25484

Reference yield:

: 5874-57-7
R-(-)-serine methyl ester hydrochloride

: 119153-86-5
C₁₆H₂₁NO₆

: 155225-25-5
N--(R)-serine methylester

Guidance literature:: With 4-methyl-morpholine; In ethyl acetate; at -15 - 20 ℃; for 13h; Yield given;
DOI:10.1016/S0957-4166(00)80107-X

Reference yield:

: 501-53-1,94274-21-2
benzyl chloroformate

: 155225-25-5
N--(R)-serine methylester

Guidance literature:: Multi-step reaction with 2 steps

1: sodium carbonate / water / 16 h / 28 °C

2: triethylamine; N-[(dimethylamino)-3-oxo-1H-1,2,3-triazolo[4,5-b]pyridin-1-yl-methylene]-N-methylmethanaminium hexafluorophosphate / N,N-dimethyl-formamide / 3 h / 20 °C

With sodium carbonate; triethylamine; N-[(dimethylamino)-3-oxo-1H-1,2,3-triazolo[4,5-b]pyridin-1-yl-methylene]-N-methylmethanaminium hexafluorophosphate; In water; N,N-dimethyl-formamide;