1-acetyl-3⁽⁵⁾-acetylamino-5⁽³⁾-(2,4-dichlorobenzylthio)-1,2,4-triazole

Base Information

Chemical Name:1-acetyl-3⁽⁵⁾-acetylamino-5⁽³⁾-(2,4-dichlorobenzylthio)-1,2,4-triazole
CAS No.:349142-05-8
Molecular Formula:C₁₃H₁₂Cl₂N₄O₂S
Molecular Weight:359.236
Hs Code.:

1-acetyl-3<sup>(5)</sup>-acetylamino-5<sup>(3)</sup>-(2,4-dichlorobenzylthio)-1,2,4-triazole

Synonyms:1-acetyl-3⁽⁵⁾-acetylamino-5⁽³⁾-(2,4-dichlorobenzylthio)-1,2,4-triazole

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1-acetyl-3⁽⁵⁾-acetylamino-5⁽³⁾-(2,4-dichlorobenzylthio)-1,2,4-triazole

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Technology Process of 1-acetyl-3⁽⁵⁾-acetylamino-5⁽³⁾-(2,4-dichlorobenzylthio)-1,2,4-triazole

There total 1 articles about 1-acetyl-3⁽⁵⁾-acetylamino-5⁽³⁾-(2,4-dichlorobenzylthio)-1,2,4-triazole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 73.0%

: 108-24-7
acetic anhydride

: 303150-34-7
5-(2,4-dichloro-benzylsulfanyl)-2H-[1,2,4]triazol-3-ylamine

: 349142-05-8
1-acetyl-3⁽⁵⁾-acetylamino-5⁽³⁾-(2,4-dichlorobenzylthio)-1,2,4-triazole

Guidance literature:: Heating;

Reference yield: 81.0%

: 349142-05-8
1-acetyl-3⁽⁵⁾-acetylamino-5⁽³⁾-(2,4-dichlorobenzylthio)-1,2,4-triazole

: 341936-97-8
3⁽⁵⁾-acetylamino-5⁽³⁾-(2,4-dichlorobenzylthio)-1,2,4-triazole

Guidance literature:: With sodium hydroxide; In water; Heating;

Reference yield:

: 349142-05-8
1-acetyl-3⁽⁵⁾-acetylamino-5⁽³⁾-(2,4-dichlorobenzylthio)-1,2,4-triazole

: 3⁽⁵⁾-acetylamino-5⁽³⁾-(2,4-dichlorobenzylsulfonyl)-1,2,4-triazole

Guidance literature:: Multi-step reaction with 2 steps

1: 81 percent / NaOH / H₂O / Heating

2: 66 percent / Na₂WO₄; H₂SO₄; H₂O₂ / acetic acid / 3 h / 60 - 85 °C

With sodium hydroxide; sodium tungstate; sulfuric acid; dihydrogen peroxide; In water; acetic acid;