benzyl 4-(6-chloro-3-(2-methoxy-2-oxoethyl)benzofuran-5-yloxy)nicotinate

Base Information

Chemical Name:benzyl 4-(6-chloro-3-(2-methoxy-2-oxoethyl)benzofuran-5-yloxy)nicotinate
CAS No.:1618131-78-4
Molecular Formula:C₂₄H₁₈ClNO₆
Molecular Weight:451.863
Hs Code.:

Synonyms:benzyl 4-(6-chloro-3-(2-methoxy-2-oxoethyl)benzofuran-5-yloxy)nicotinate

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Chemical Property of benzyl 4-(6-chloro-3-(2-methoxy-2-oxoethyl)benzofuran-5-yloxy)nicotinate

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Technology Process of benzyl 4-(6-chloro-3-(2-methoxy-2-oxoethyl)benzofuran-5-yloxy)nicotinate

There total 3 articles about benzyl 4-(6-chloro-3-(2-methoxy-2-oxoethyl)benzofuran-5-yloxy)nicotinate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 78.0%

: 1618131-28-4
benzyl 4-chloronicotinate

: 1618131-96-6
methyl 2-(6-chloro-5-hydroxybenzofuran-3-yl)acetate

: 1618131-78-4
benzyl 4-(6-chloro-3-(2-methoxy-2-oxoethyl)benzofuran-5-yloxy)nicotinate

Guidance literature:: With potassium carbonate; In N,N-dimethyl-formamide; at 110 ℃;
DOI:10.1016/j.ejmech.2014.05.031

Reference yield:

: 10177-29-4
4-chloronicotinic acid

: 1618131-78-4
benzyl 4-(6-chloro-3-(2-methoxy-2-oxoethyl)benzofuran-5-yloxy)nicotinate

Guidance literature:: Multi-step reaction with 2 steps

1.1: triethylamine; thionyl chloride / N,N-dimethyl-formamide; dichloromethane / 2 h / Reflux

1.2: 20 °C

2.1: potassium carbonate / N,N-dimethyl-formamide / 110 °C

With thionyl chloride; potassium carbonate; triethylamine; In dichloromethane; N,N-dimethyl-formamide;
DOI:10.1016/j.ejmech.2014.05.031

Reference yield:

: 100-51-6,185532-71-2
benzyl alcohol

: 1618131-78-4
benzyl 4-(6-chloro-3-(2-methoxy-2-oxoethyl)benzofuran-5-yloxy)nicotinate

Guidance literature:: Multi-step reaction with 2 steps

1.1: triethylamine; thionyl chloride / N,N-dimethyl-formamide; dichloromethane / 2 h / Reflux

1.2: 20 °C

2.1: potassium carbonate / N,N-dimethyl-formamide / 110 °C

With thionyl chloride; potassium carbonate; triethylamine; In dichloromethane; N,N-dimethyl-formamide;
DOI:10.1016/j.ejmech.2014.05.031