2-{[(6-morpholin-4-ylpyridin-3-yl)amino]acetyl}-N-phenylhydrazinecarbothioamide

Base Information

Chemical Name:2-{[(6-morpholin-4-ylpyridin-3-yl)amino]acetyl}-N-phenylhydrazinecarbothioamide
CAS No.:1415835-22-1
Molecular Formula:C₁₈H₂₂N₆O₂S
Molecular Weight:386.478
Hs Code.:

Synonyms:2-{[(6-morpholin-4-ylpyridin-3-yl)amino]acetyl}-N-phenylhydrazinecarbothioamide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2-{[(6-morpholin-4-ylpyridin-3-yl)amino]acetyl}-N-phenylhydrazinecarbothioamide

Chemical Property:

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Technology Process of 2-{[(6-morpholin-4-ylpyridin-3-yl)amino]acetyl}-N-phenylhydrazinecarbothioamide

There total 3 articles about 2-{[(6-morpholin-4-ylpyridin-3-yl)amino]acetyl}-N-phenylhydrazinecarbothioamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

: 1415835-17-4
2-[6-(morpholin-4-yl)pyridin-3-ylamino]acetohydrazide

: 103-72-0
phenyl isothiocyanate

: 1415835-22-1
2-{[(6-morpholin-4-ylpyridin-3-yl)amino]acetyl}-N-phenylhydrazinecarbothioamide

Guidance literature:: In ethanol; for 6h; Reflux;
DOI:10.1007/s00044-012-0318-1

Reference yield:

: 1415835-16-3
ethyl N-(6-morpholin-4-ylpyridin-3-yl)glycinate

: 1415835-22-1
2-{[(6-morpholin-4-ylpyridin-3-yl)amino]acetyl}-N-phenylhydrazinecarbothioamide

Guidance literature:: Multi-step reaction with 2 steps

1: hydrazine hydrate / ethanol / 7 h / Reflux

2: ethanol / 6 h / Reflux

With hydrazine hydrate; In ethanol;
DOI:10.1007/s00044-012-0318-1

Reference yield:

: 52023-68-4
6-(morpholin-4-yl)pyridin-3-amine

: 1415835-22-1
2-{[(6-morpholin-4-ylpyridin-3-yl)amino]acetyl}-N-phenylhydrazinecarbothioamide

Guidance literature:: Multi-step reaction with 3 steps

1: triethylamine / tetrahydrofuran / 11 h / 20 °C

2: hydrazine hydrate / ethanol / 7 h / Reflux

3: ethanol / 6 h / Reflux

With hydrazine hydrate; triethylamine; In tetrahydrofuran; ethanol;
DOI:10.1007/s00044-012-0318-1