C₃₂H₂₈N₂O₃

Base Information

Chemical Name:C₃₂H₂₈N₂O₃
CAS No.:1418140-82-5
Molecular Formula:C₃₂H₂₈N₂O₃
Molecular Weight:488.586
Hs Code.:

C<sub>32</sub>H<sub>28</sub>N<sub>2</sub>O<sub>3</sub>

Synonyms:C₃₂H₂₈N₂O₃

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Chemical Property of C₃₂H₂₈N₂O₃

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Technology Process of C₃₂H₂₈N₂O₃

There total 13 articles about C₃₂H₂₈N₂O₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₃₃H₃₀N₂O₃

: 1418140-82-5
C₃₂H₂₈N₂O₃

Guidance literature:: With water; sodium hydroxide; In tetrahydrofuran; methanol; at 20 ℃; for 12h;
DOI:10.1016/j.bmcl.2012.11.033

Reference yield:

: 183007-32-1
4-benzyloxy-1-iodo-2-nitrobenzene

: 1418140-82-5
C₃₂H₂₈N₂O₃

Guidance literature:: Multi-step reaction with 9 steps

1.1: palladium diacetate; Tri(p-tolyl)phosphine; triethylamine / acetonitrile / 0.5 h / 20 °C / Inert atmosphere

1.2: 20 °C / Reflux

2.1: zinc; acetic acid / 1 h / 20 °C

3.1: pyridine / dichloromethane / 0.5 h / 20 °C

3.2: 20 °C

4.1: triethylamine; bis(trichloromethyl) carbonate / dichloromethane / 3 h / 0 - 20 °C / Inert atmosphere

5.1: tri-n-butyl-tin hydride; 2,2'-azobis(isobutyronitrile) / toluene / 3.5 h / 20 - 80 °C / Inert atmosphere

6.1: 10 wt% Pd(OH)2 on carbon; hydrogen / methanol; acetic acid / 3 h / 20 °C / 760.05 Torr / Inert atmosphere

7.1: 1,1'-azodicarbonyl-dipiperidine; tributylphosphine / tetrahydrofuran; toluene / 3 h / 20 °C

8.1: sodium hydride / tetrahydrofuran; mineral oil / 2 h / 20 °C

9.1: sodium hydroxide; water / tetrahydrofuran; methanol / 12 h / 20 °C

With pyridine; 2,2'-azobis(isobutyronitrile); tributylphosphine; bis(trichloromethyl) carbonate; 10 wt% Pd(OH)2 on carbon; water; hydrogen; tri-n-butyl-tin hydride; palladium diacetate; sodium hydride; acetic acid; triethylamine; Tri(p-tolyl)phosphine; sodium hydroxide; zinc; 1,1'-azodicarbonyl-dipiperidine; In tetrahydrofuran; methanol; dichloromethane; acetic acid; toluene; acetonitrile; mineral oil;
DOI:10.1016/j.bmcl.2012.11.033

Reference yield:

: 113305-56-9
4-iodo-3-nitrophenol

: 1418140-82-5
C₃₂H₂₈N₂O₃

Guidance literature:: Multi-step reaction with 10 steps

1.1: potassium carbonate / acetone

2.1: palladium diacetate; Tri(p-tolyl)phosphine; triethylamine / acetonitrile / 0.5 h / 20 °C / Inert atmosphere

2.2: 20 °C / Reflux

3.1: zinc; acetic acid / 1 h / 20 °C

4.1: pyridine / dichloromethane / 0.5 h / 20 °C

4.2: 20 °C

5.1: triethylamine; bis(trichloromethyl) carbonate / dichloromethane / 3 h / 0 - 20 °C / Inert atmosphere

6.1: tri-n-butyl-tin hydride; 2,2'-azobis(isobutyronitrile) / toluene / 3.5 h / 20 - 80 °C / Inert atmosphere

7.1: 10 wt% Pd(OH)2 on carbon; hydrogen / methanol; acetic acid / 3 h / 20 °C / 760.05 Torr / Inert atmosphere

8.1: 1,1'-azodicarbonyl-dipiperidine; tributylphosphine / tetrahydrofuran; toluene / 3 h / 20 °C

9.1: sodium hydride / tetrahydrofuran; mineral oil / 2 h / 20 °C

10.1: sodium hydroxide; water / tetrahydrofuran; methanol / 12 h / 20 °C

With pyridine; 2,2'-azobis(isobutyronitrile); tributylphosphine; bis(trichloromethyl) carbonate; 10 wt% Pd(OH)2 on carbon; water; hydrogen; tri-n-butyl-tin hydride; palladium diacetate; sodium hydride; potassium carbonate; acetic acid; triethylamine; Tri(p-tolyl)phosphine; sodium hydroxide; zinc; 1,1'-azodicarbonyl-dipiperidine; In tetrahydrofuran; methanol; dichloromethane; acetic acid; acetone; toluene; acetonitrile; mineral oil;
DOI:10.1016/j.bmcl.2012.11.033