Carbonic acid 4-((5R,5aR,8aS)-9-azido-6-oxo-5,5a,6,8,8a,9-hexahydro-furo[3',4':6,7]naphtho[2,3-d][1,3]dioxol-5-yl)-2,6-dimethoxy-phenyl ester benzyl ester

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Chemical Name:Carbonic acid 4-((5R,5aR,8aS)-9-azido-6-oxo-5,5a,6,8,8a,9-hexahydro-furo[3',4':6,7]naphtho[2,3-d][1,3]dioxol-5-yl)-2,6-dimethoxy-phenyl ester benzyl ester
CAS No.:197016-30-1
Molecular Formula:C₂₉H₂₅N₃O₉
Molecular Weight:559.532
Hs Code.:

Synonyms:Carbonic acid 4-((5R,5aR,8aS)-9-azido-6-oxo-5,5a,6,8,8a,9-hexahydro-furo[3',4':6,7]naphtho[2,3-d][1,3]dioxol-5-yl)-2,6-dimethoxy-phenyl ester benzyl ester

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Chemical Property of Carbonic acid 4-((5R,5aR,8aS)-9-azido-6-oxo-5,5a,6,8,8a,9-hexahydro-furo[3',4':6,7]naphtho[2,3-d][1,3]dioxol-5-yl)-2,6-dimethoxy-phenyl ester benzyl ester

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Technology Process of Carbonic acid 4-((5R,5aR,8aS)-9-azido-6-oxo-5,5a,6,8,8a,9-hexahydro-furo[3',4':6,7]naphtho[2,3-d][1,3]dioxol-5-yl)-2,6-dimethoxy-phenyl ester benzyl ester

There total 6 articles about Carbonic acid 4-((5R,5aR,8aS)-9-azido-6-oxo-5,5a,6,8,8a,9-hexahydro-furo[3',4':6,7]naphtho[2,3-d][1,3]dioxol-5-yl)-2,6-dimethoxy-phenyl ester benzyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

: 501-53-1,94274-21-2
benzyl chloroformate

: (5R,5aR,8aS)-9-Azido-5-(4-hydroxy-3,5-dimethoxy-phenyl)-5,8,8a,9-tetrahydro-5aH-furo[3',4':6,7]naphtho[2,3-d][1,3]dioxol-6-one

: 197016-30-1
Carbonic acid 4-((5R,5aR,8aS)-9-azido-6-oxo-5,5a,6,8,8a,9-hexahydro-furo[3',4':6,7]naphtho[2,3-d][1,3]dioxol-5-yl)-2,6-dimethoxy-phenyl ester benzyl ester

Guidance literature:: With pyridine; In dichloromethane; at 0 ℃; for 15h;

Reference yield: 34.0%

: C₃₀H₂₈O₁₂S

: 197016-30-1
Carbonic acid 4-((5R,5aR,8aS)-9-azido-6-oxo-5,5a,6,8,8a,9-hexahydro-furo[3',4':6,7]naphtho[2,3-d][1,3]dioxol-5-yl)-2,6-dimethoxy-phenyl ester benzyl ester

Guidance literature:: With sodium azide; In N,N-dimethyl-formamide; at 0 - 20 ℃; for 4h;

Reference yield:

: 6559-91-7
4'-demethylepipodophyllotoxin

: 197016-30-1
Carbonic acid 4-((5R,5aR,8aS)-9-azido-6-oxo-5,5a,6,8,8a,9-hexahydro-furo[3',4':6,7]naphtho[2,3-d][1,3]dioxol-5-yl)-2,6-dimethoxy-phenyl ester benzyl ester

Guidance literature:: Multi-step reaction with 3 steps

2: Et₃N

3: NaN₃

With sodium azide; triethylamine;
DOI:10.1016/S0040-4039(97)01582-7