[rhodium(I)((Ph₂P)2N-C₆H₄-2-CH(CH₃)2)(1,5-cyclooctadiene)](tetrafluoroborate)

Base Information

• Chemical Name: [rhodium(I)((Ph₂P)2N-C₆H₄-2-CH(CH₃)2)(1,5-cyclooctadiene)](tetrafluoroborate)
• CAS No.: 1428246-98-3
• Molecular Formula: BF₄*C₄₁H₄₃NP₂Rh
• Molecular Weight: 801.457

Synonyms:[rhodium(I)((Ph₂P)2N-C₆H₄-2-CH(CH₃)2)(1,5-cyclooctadiene)](tetrafluoroborate)

Chemical Property of [rhodium(I)((Ph₂P)2N-C₆H₄-2-CH(CH₃)2)(1,5-cyclooctadiene)](tetrafluoroborate)

Chemical Property:

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Technology Process of [rhodium(I)((Ph₂P)2N-C₆H₄-2-CH(CH₃)2)(1,5-cyclooctadiene)](tetrafluoroborate)

There total 1 articles about [rhodium(I)((Ph₂P)2N-C₆H₄-2-CH(CH₃)2)(1,5-cyclooctadiene)](tetrafluoroborate) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.2%

bis(1,5-cyclooctadiene)rhodium(I) tetrafluoroborate (35138-22-8) + N,N-bis(diphenylphosphino)-2-isopropylaniline (1012318-48-7) → [rhodium(I)((Ph2P)2N-C6H4-2-CH(CH3)2)(1,5-cyclooctadiene)](tetrafluoroborate) (1428246-98-3)

Guidance literature:

In tetrahydrofuran; at 25 ℃; for 0.5h; Inert atmosphere; Schlenk technique;

DOI:10.1016/j.ica.2012.12.005

Reference yield:

N,N-bis(diphenylphosphino)-2-isopropylaniline (1012318-48-7) + [rhodium(I)((Ph2P)2N-C6H4-2-CH(CH3)2)(1,5-cyclooctadiene)](tetrafluoroborate) (1428246-98-3) → [rhodium(I)((Ph2P)2N-C6H4-2-CH(CH3)2)2](tetrafluoroborate)

Guidance literature:

In tetrahydrofuran; at 25 ℃; for 6h; Inert atmosphere; Schlenk technique;

DOI:10.1016/j.ica.2012.12.005

upstream raw materials:

bis(1,5-cyclooctadiene)rhodium(I) tetrafluoroborate

N,N-bis(diphenylphosphino)-2-isopropylaniline

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