Technology Process of C9H9N3O4
There total 8 articles about C9H9N3O4 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
sodium hydroxide;
In
methanol; water;
for 2h;
Reflux;
DOI:10.1039/c4ob00923a
- Guidance literature:
-
Multi-step reaction with 5 steps
1: hydrogenchloride / water / 2 h / 100 °C
2: sulfuric acid / 2 h / Reflux
3: palladium on activated charcoal; ammonium formate / methanol / 20 °C
4: trimethylsilylazide; tert.-butylnitrite / acetonitrile / 2 h / Cooling with ice
5: sodium hydroxide / water; methanol / 2 h / Reflux
With
hydrogenchloride; tert.-butylnitrite; trimethylsilylazide; sulfuric acid; palladium on activated charcoal; ammonium formate; sodium hydroxide;
In
methanol; water; acetonitrile;
DOI:10.1039/c4ob00923a
- Guidance literature:
-
Multi-step reaction with 8 steps
1: nitric acid; acetic acid / 3 h / 0 °C
2: potassium carbonate / N,N-dimethyl-formamide / 5 h / 0 - 20 °C
3: acetonitrile / 20 °C
4: hydrogenchloride / water / 2 h / 100 °C
5: sulfuric acid / 2 h / Reflux
6: palladium on activated charcoal; ammonium formate / methanol / 20 °C
7: trimethylsilylazide; tert.-butylnitrite / acetonitrile / 2 h / Cooling with ice
8: sodium hydroxide / water; methanol / 2 h / Reflux
With
hydrogenchloride; tert.-butylnitrite; trimethylsilylazide; sulfuric acid; palladium on activated charcoal; nitric acid; ammonium formate; potassium carbonate; acetic acid; sodium hydroxide;
In
methanol; water; N,N-dimethyl-formamide; acetonitrile;
DOI:10.1039/c4ob00923a
