ethyl 2-{5-[2-(benzyloxy)-4-methylpentyl]tetrahydrofuran-2-yl}-2-bromopropanoate

Base Information

Chemical Name:ethyl 2-{5-[2-(benzyloxy)-4-methylpentyl]tetrahydrofuran-2-yl}-2-bromopropanoate
CAS No.:1095268-56-6
Molecular Formula:C₂₂H₃₃BrO₄
Molecular Weight:441.406
Hs Code.:

Synonyms:ethyl 2-{5-[2-(benzyloxy)-4-methylpentyl]tetrahydrofuran-2-yl}-2-bromopropanoate

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Chemical Property of ethyl 2-{5-[2-(benzyloxy)-4-methylpentyl]tetrahydrofuran-2-yl}-2-bromopropanoate

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Technology Process of ethyl 2-{5-[2-(benzyloxy)-4-methylpentyl]tetrahydrofuran-2-yl}-2-bromopropanoate

There total 1 articles about ethyl 2-{5-[2-(benzyloxy)-4-methylpentyl]tetrahydrofuran-2-yl}-2-bromopropanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 1095268-55-5
ethyl (2E,6S,8S)-8-(benzyloxy)-6-(2,6-dichlorobenzyloxy)-2,10-dimethylundec-2-enoate

: 1095268-56-6
ethyl 2-{5-[2-(benzyloxy)-4-methylpentyl]tetrahydrofuran-2-yl}-2-bromopropanoate

Guidance literature:: With bromine; In dichloromethane; at -78 ℃; for 1h; Inert atmosphere; Darkness;
DOI:10.1016/j.tet.2008.09.038

Reference yield: 85.0%

: 1095268-56-6
ethyl 2-{5-[2-(benzyloxy)-4-methylpentyl]tetrahydrofuran-2-yl}-2-bromopropanoate

: ethyl 2-{5-[2-(benzyloxy)-4-methylpentyl]-tetrahydrofuran-2-yl}propanoate

: 1095268-57-7
ethyl 2-{5-[2-(benzyloxy)-4-methylpentyl]-tetrahydrofuran-2-yl}propanoate

Guidance literature:: With 2,2'-azobis(isobutyronitrile); tris-(trimethylsilyl)silane; In toluene; at -25 ℃; for 1.5h; optical yield given as %de; Inert atmosphere; UV-irradiation;
DOI:10.1016/j.tet.2008.09.038