C₂₂H₂₁N₃O₄

Base Information

Chemical Name:C₂₂H₂₁N₃O₄
CAS No.:1332848-35-7
Molecular Formula:C₂₂H₂₁N₃O₄
Molecular Weight:391.426
Hs Code.:

C<sub>22</sub>H<sub>21</sub>N<sub>3</sub>O<sub>4</sub>

Synonyms:C₂₂H₂₁N₃O₄

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Chemical Property of C₂₂H₂₁N₃O₄

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Technology Process of C₂₂H₂₁N₃O₄

There total 1 articles about C₂₂H₂₁N₃O₄ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

: 1116188-99-8
Nα-Boc-N1-Cbz-L-tryptophan methyl ester

: 15761-38-3
L-N-Boc-Ala

: 1332848-35-7
C₂₂H₂₁N₃O₄

Guidance literature:: Nα-Boc-N1-Cbz-L-tryptophan methyl ester; With trifluoroacetic acid; In dichloromethane; at 23 ℃; for 1h; Inert atmosphere;

L-N-Boc-Ala; With benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; In dichloromethane; at 0 - 23 ℃; for 13.5h; Further stages; Inert atmosphere;
DOI:10.1021/ja206743v

Reference yield: 69.2%

: 1332848-35-7
C₂₂H₂₁N₃O₄

: 1332848-37-9
C₂₂H₂₀BrN₃O₄

Guidance literature:: With pyridinium hydrobromide perbromide; In 2,2,2-trifluoroethanol; at 23 ℃; for 0.333333h; Inert atmosphere;
DOI:10.1021/ja206743v

Reference yield:

: 1332848-35-7
C₂₂H₂₁N₃O₄

: 1332848-47-1
C₂₅H₂₅N₃O₄

Guidance literature:: Multi-step reaction with 2 steps

1: pyridinium hydrobromide perbromide / 2,2,2-trifluoroethanol / 0.33 h / 23 °C / Inert atmosphere

2: silver hexafluoroantimonate; 18-crown-6 ether / dichloromethane / 1 h / 23 °C / Inert atmosphere

With silver hexafluoroantimonate; pyridinium hydrobromide perbromide; 18-crown-6 ether; In dichloromethane; 2,2,2-trifluoroethanol;
DOI:10.1021/ja206743v