3-(2-deoxy-beta-D-erythro-pentofuranosyl)-6,7-dihydroxy-3,4,6,7-tetrahydro-9H-imidazo[1,2-a]purin-9-one

Base Information

• Chemical Name: 3-(2-deoxy-beta-D-erythro-pentofuranosyl)-6,7-dihydroxy-3,4,6,7-tetrahydro-9H-imidazo[1,2-a]purin-9-one
• CAS No.: 99508-95-9
• Molecular Formula: C₁₂H₁₅N₅O₆
• Molecular Weight: 325.281

Synonyms:3-(2-deoxy-β-D-erythropentofuranosyl)-6,7-dihydro-6,7-dihydroxyimidazo<1,2-a>purin-9(3H)-one

Chemical Property of 3-(2-deoxy-beta-D-erythro-pentofuranosyl)-6,7-dihydroxy-3,4,6,7-tetrahydro-9H-imidazo[1,2-a]purin-9-one

Chemical Property:

• Vapor Pressure: 1.09E-25mmHg at 25°C

Purity/Quality:

99% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 3-(2-deoxy-beta-D-erythro-pentofuranosyl)-6,7-dihydroxy-3,4,6,7-tetrahydro-9H-imidazo[1,2-a]purin-9-one

There total 4 articles about 3-(2-deoxy-beta-D-erythro-pentofuranosyl)-6,7-dihydroxy-3,4,6,7-tetrahydro-9H-imidazo[1,2-a]purin-9-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

2'-Deoxyguanosine (961-07-9) + 2-Amino-1-methyl-4,5-dihydro-1H-imidazole-4,5-diol (124762-93-2,124762-94-3) → 1-methylguanidine (471-29-4) + 3-(2-deoxy-β-D-erythropentofuranosyl)-6,7-dihydro-6,7-dihydroxyimidazo<1,2-a>purin-9(3H)-one (99508-95-9)

Guidance literature:

at 25 ℃; Equilibrium constant; 0.05 M phosphate buffer, pH 7.5;

DOI:10.1139/v89-331

Reference yield:

1,N2-etheno-2′-deoxyguanosine (108929-11-9) → 2'-Deoxyguanosine (961-07-9) + 3-(2-deoxy-β-D-erythropentofuranosyl)-6,7-dihydro-6,7-dihydroxyimidazo<1,2-a>purin-9(3H)-one (99508-95-9)

Guidance literature:

With oxygen; N-(2,3-dihydroxy-propyl)-3-{8-[2-(2,3-dihydroxypropylcarbamoyl)-ethyl]-9,10-dioxa-tricyclo[6.2.2.0^2,7]-dodeca-2,4,6,11-tetraen-1-yl}-propionamide;

DOI:10.1515/hsz-2017-0337

Reference yield:

2-Bromo-malonaldehyde (2065-75-0) + 2'-Deoxyguanosine (961-07-9) → 3-(2-deoxy-β-D-erythropentofuranosyl)-6,7-dihydro-6,7-dihydroxyimidazo<1,2-a>purin-9(3H)-one (99508-95-9) + 1,N2-etheno-2′-deoxyguanosine (108929-11-9) + 1,N2-(2-formyl-1,2,3-trihydroxypropano)-2'-deoxyguanosine + 1,N2-(1,2,2,3-tetrahydroxypropano)-2'-deoxyguanosine

Guidance literature:

In various solvent(s); at 60 ℃; pH=7.4; Title compound not separated from byproducts;

DOI:10.1039/b405117c

upstream raw materials:

2'-Deoxyguanosine

2-Amino-1-methyl-4,5-dihydro-1H-imidazole-4,5-diol

2-Bromo-malonaldehyde

1,N²-etheno-2′-deoxyguanosine

Downstream raw materials:

2'-Deoxyguanosine

2-Amino-1-(2-hydroxy-3-methoxy-propyl)-4,5-dihydro-1H-imidazole-4,5-diol

2-Amino-1-methyl-4,5-dihydro-1H-imidazole-4,5-diol

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