Bicyclo<4.4.1>undeca-4,6,8,10-tetraen-2,3-dion-2-<(4-chlorphenyl)hydrazon>

Base Information

Chemical Name:Bicyclo<4.4.1>undeca-4,6,8,10-tetraen-2,3-dion-2-<(4-chlorphenyl)hydrazon>
CAS No.:86226-29-1
Molecular Formula:C₁₇H₁₃ClN₂O
Molecular Weight:296.756
Hs Code.:

Synonyms:Bicyclo<4.4.1>undeca-4,6,8,10-tetraen-2,3-dion-2-<(4-chlorphenyl)hydrazon>

Suppliers and Price of Bicyclo<4.4.1>undeca-4,6,8,10-tetraen-2,3-dion-2-<(4-chlorphenyl)hydrazon>

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Bicyclo<4.4.1>undeca-4,6,8,10-tetraen-2,3-dion-2-<(4-chlorphenyl)hydrazon>

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Technology Process of Bicyclo<4.4.1>undeca-4,6,8,10-tetraen-2,3-dion-2-<(4-chlorphenyl)hydrazon>

There total 2 articles about Bicyclo<4.4.1>undeca-4,6,8,10-tetraen-2,3-dion-2-<(4-chlorphenyl)hydrazon> which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 78.0%

: 17333-85-6
4-chlorophenyldiazonium salt

: 86226-25-7
3-tert-butoxy-1,6-methano<10>annulen

: 86226-29-1
Bicyclo<4.4.1>undeca-4,6,8,10-tetraen-2,3-dion-2-<(4-chlorphenyl)hydrazon>

Guidance literature:: With sulfuric acid; In acetic acid;
DOI:10.1246/cl.1983.653

Reference yield:

: 86226-25-7
3-tert-butoxy-1,6-methano<10>annulen

: 106-47-8
4-chloro-aniline

: 86226-29-1
Bicyclo<4.4.1>undeca-4,6,8,10-tetraen-2,3-dion-2-<(4-chlorphenyl)hydrazon>

Guidance literature:: With sulfuric acid; sodium nitrite; Yield given. Multistep reaction; 1.) glacial acetic acid, H₂O, 0 deg C, 2.) glacial acetic acid, room temp.;