2-R-hydroxysuccinic acid 1-benzylester

Base Information

• Chemical Name: 2-R-hydroxysuccinic acid 1-benzylester
• CAS No.: 83477-74-1
• Molecular Formula: C₁₁H₁₂O₅
• Molecular Weight: 224.213

Synonyms:2-R-hydroxysuccinic acid 1-benzylester

Chemical Property of 2-R-hydroxysuccinic acid 1-benzylester

Chemical Property:

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Technology Process of 2-R-hydroxysuccinic acid 1-benzylester

There total 4 articles about 2-R-hydroxysuccinic acid 1-benzylester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

benzyl alcohol (100-51-6,185532-71-2) → 2-R-hydroxysuccinic acid 1-benzylester (83477-74-1)

Guidance literature:

D-Malic acid; With trifluoromethylsulfonic anhydride; at 20 ℃; for 2h;

benzyl alcohol; at 20 ℃;

Reference yield: 92.0%

D-Malic acid (636-61-3,78644-42-5) + benzyl alcohol (100-51-6,185532-71-2) → 2-R-hydroxysuccinic acid 1-benzylester (83477-74-1)

Guidance literature:

With trifluoroacetic anhydride; Inert atmosphere;

DOI:10.1021/acs.jnatprod.8b01083

Reference yield:

(R)-3-Hydroxy-dihydro-furan-2,5-dione (1121-34-2) + benzyl alcohol (100-51-6,185532-71-2) → 2-R-hydroxysuccinic acid 1-benzylester (83477-74-1)

Guidance literature:

In tetrahydrofuran; Yield given;

DOI:10.1021/jo00146a020

upstream raw materials:

(R)-3-Hydroxy-dihydro-furan-2,5-dione

benzyl alcohol

(R)-2,5-dioxotetrahydrofuran-3-yl 2,2,2-trifluoroacetate

D-Malic acid

Downstream raw materials:

(R)-2-oxo-oxazolidine-5-carboxylic acid benzyl ester

2-R-hydroxysuccinic acid-1-benzylester-4-(4-methoxybenzyl) ester

(R)-3-acetoxy-3-benzyloxycarbonyl propionic acid

(S)-1-Benzyloxy-4-oxo-azetidine-2-carboxylic acid benzyl ester

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