4-(diphenyloxophosphanyl)-1-(1,3-diethyl-1,3,2-benzodiazaborol-2-yl)benzene

Base Information

Chemical Name:4-(diphenyloxophosphanyl)-1-(1,3-diethyl-1,3,2-benzodiazaborol-2-yl)benzene
CAS No.:1394158-89-4
Molecular Formula:C₂₈H₂₈BN₂OP
Molecular Weight:450.328
Hs Code.:

Synonyms:4-(diphenyloxophosphanyl)-1-(1,3-diethyl-1,3,2-benzodiazaborol-2-yl)benzene

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Chemical Property of 4-(diphenyloxophosphanyl)-1-(1,3-diethyl-1,3,2-benzodiazaborol-2-yl)benzene

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Technology Process of 4-(diphenyloxophosphanyl)-1-(1,3-diethyl-1,3,2-benzodiazaborol-2-yl)benzene

There total 3 articles about 4-(diphenyloxophosphanyl)-1-(1,3-diethyl-1,3,2-benzodiazaborol-2-yl)benzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 65.0%

: 37222-66-5,70693-62-8,10058-23-8
Oxone

: 1394158-87-2
4-(diphenylphosphanyl)-1-(1,3-diethyl-1,3,2-benzodiazaborol-2-yl)benzene

: 1394158-89-4
4-(diphenyloxophosphanyl)-1-(1,3-diethyl-1,3,2-benzodiazaborol-2-yl)benzene

Guidance literature:: With silica gel; In toluene; at 110 ℃; for 72h; Inert atmosphere; Schlenk technique;
DOI:10.1039/c2dt30666b

Reference yield:

: 383913-07-3
2-bromo-1,3-diethyl-2,3-dihydro-1H-1,3,2-benzodiazoborole

: 1394158-89-4
4-(diphenyloxophosphanyl)-1-(1,3-diethyl-1,3,2-benzodiazaborol-2-yl)benzene

Guidance literature:: Multi-step reaction with 2 steps

1.1: tert.-butyl lithium / diethyl ether; hexane / 3 h / -78 - -60 °C / Inert atmosphere; Schlenk technique

1.2: -78 - 20 °C / Schlenk technique; Inert atmosphere

2.1: silica gel / toluene / 72 h / 110 °C / Inert atmosphere; Schlenk technique

With tert.-butyl lithium; silica gel; In diethyl ether; hexane; toluene;
DOI:10.1039/c2dt30666b

Reference yield:

: 734-59-8
(4-bromophenyl)diphenylphosphane

: 1394158-89-4
4-(diphenyloxophosphanyl)-1-(1,3-diethyl-1,3,2-benzodiazaborol-2-yl)benzene

Guidance literature:: Multi-step reaction with 2 steps

1.1: tert.-butyl lithium / diethyl ether; hexane / 3 h / -78 - -60 °C / Inert atmosphere; Schlenk technique

1.2: -78 - 20 °C / Schlenk technique; Inert atmosphere

2.1: silica gel / toluene / 72 h / 110 °C / Inert atmosphere; Schlenk technique

With tert.-butyl lithium; silica gel; In diethyl ether; hexane; toluene;
DOI:10.1039/c2dt30666b