C₃₁H₃₁N₇O₃

Base Information

Chemical Name:C₃₁H₃₁N₇O₃
CAS No.:1312611-25-8
Molecular Formula:C₃₁H₃₁N₇O₃
Molecular Weight:549.632
Hs Code.:

C<sub>31</sub>H<sub>31</sub>N<sub>7</sub>O<sub>3</sub>

Synonyms:C₃₁H₃₁N₇O₃

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Chemical Property of C₃₁H₃₁N₇O₃

Chemical Property:

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Technology Process of C₃₁H₃₁N₇O₃

There total 14 articles about C₃₁H₃₁N₇O₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 31.0%

: 1312611-24-7
C₃₉H₃₇N₇O₅

: 1312611-25-8
C₃₁H₃₁N₇O₃

Guidance literature:: C₃₉H₃₇N₇O₅; With hydrogen bromide; acetic acid; In water; at 20 ℃; for 5h;

With sodium carbonate; In water; pH=8; Cooling with ice;

Reference yield:

: 5332-25-2
6-bromoquinoline

: 1312611-25-8
C₃₁H₃₁N₇O₃

Guidance literature:: Multi-step reaction with 11 steps

1.1: 3-chloro-benzenecarboperoxoic acid / dichloromethane / 1 h / 20 °C / Cooling with ice

2.1: chloro-trimethyl-silane; triethylamine / N,N-dimethyl-formamide / 100 °C

3.1: hydrogenchloride; water / 19 h / Reflux

4.1: triethylamine; diphenyl phosphoryl azide / N,N-dimethyl-formamide / 7 h / 100 °C

5.1: trifluoroacetic acid / dichloromethane / 5 h / 20 °C

6.1: HATU / N,N-dimethyl-formamide / 1 h / 20 °C

6.2: 20 °C

7.1: potassium acetate / (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride / 1,4-dioxane / 8 h / 100 - 110 °C

8.1: sodium carbonate / tetrakis(triphenylphosphine) palladium⁽⁰⁾ / toluene; ethanol / 80 °C / Inert atmosphere

9.1: hydrogenchloride / methanol / 2 h / 20 °C

10.1: (benzotriazo-1-yloxy)tris(dimethylamino)phosphonium hexafluorophosphate; N-ethyl-N,N-diisopropylamine / dichloromethane / 20 °C

11.1: hydrogen bromide; acetic acid / water / 5 h / 20 °C

11.2: pH 8 / Cooling with ice

With hydrogenchloride; chloro-trimethyl-silane; diphenyl phosphoryl azide; water; hydrogen bromide; potassium acetate; sodium carbonate; (benzotriazo-1-yloxy)tris(dimethylamino)phosphonium hexafluorophosphate; acetic acid; triethylamine; N-ethyl-N,N-diisopropylamine; 3-chloro-benzenecarboperoxoic acid; HATU; trifluoroacetic acid; (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In 1,4-dioxane; methanol; ethanol; dichloromethane; water; N,N-dimethyl-formamide; toluene; 8.1: Suzuki Coupling;

Reference yield:

: 1148-11-4
N-Benzyloxycarbonyl-L-proline

: 1312611-25-8
C₃₁H₃₁N₇O₃

Guidance literature:: Multi-step reaction with 6 steps

1.1: oxalyl dichloride / N,N-dimethyl-formamide / dichloromethane / 1.5 h / 20 °C

2.1: sodium hydride / N,N-dimethyl-formamide / 1 h / 0 °C

2.2: 20 °C

3.1: sodium carbonate / tetrakis(triphenylphosphine) palladium⁽⁰⁾ / toluene; ethanol / 80 °C / Inert atmosphere

4.1: hydrogenchloride / methanol / 2 h / 20 °C

5.1: (benzotriazo-1-yloxy)tris(dimethylamino)phosphonium hexafluorophosphate; N-ethyl-N,N-diisopropylamine / dichloromethane / 20 °C

6.1: hydrogen bromide; acetic acid / water / 5 h / 20 °C

6.2: pH 8 / Cooling with ice

With hydrogenchloride; oxalyl dichloride; hydrogen bromide; sodium hydride; sodium carbonate; (benzotriazo-1-yloxy)tris(dimethylamino)phosphonium hexafluorophosphate; acetic acid; N-ethyl-N,N-diisopropylamine; tetrakis(triphenylphosphine) palladium⁽⁰⁾; N,N-dimethyl-formamide; In methanol; ethanol; dichloromethane; water; N,N-dimethyl-formamide; toluene; 3.1: Suzuki Coupling;